C₁₉H₁₃BrF₃N₃O₂

Base Information

Chemical Name:C₁₉H₁₃BrF₃N₃O₂
CAS No.:1350327-52-4
Molecular Formula:C₁₉H₁₃BrF₃N₃O₂
Molecular Weight:452.23
Hs Code.:

C<sub>19</sub>H<sub>13</sub>BrF<sub>3</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₁₉H₁₃BrF₃N₃O₂

Chemical Property:

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Technology Process of C₁₉H₁₃BrF₃N₃O₂

There total 4 articles about C₁₉H₁₃BrF₃N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 888327-38-6
2,4-dichloro-5-(trifluoromethyl)pyridine

: 1350327-52-4
C₁₉H₁₃BrF₃N₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 1 h / 130 °C / Microwave irradiation

2: palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 12 h / 120 °C / Microwave irradiation

3: dihydrogen peroxide; potassium hydroxide / ethanol; dimethyl sulfoxide

With dihydrogen peroxide; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium hydroxide; In 1,4-dioxane; ethanol; dimethyl sulfoxide; 1: Buchwald amination / 2: Buchwald amination;
DOI:10.1016/j.bmcl.2011.09.090

Reference yield:

: C₁₃H₇ClF₃N₃

: 1350327-52-4
C₁₉H₁₃BrF₃N₃O₂

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene / 1,4-dioxane / 12 h / 120 °C / Microwave irradiation

2: dihydrogen peroxide; potassium hydroxide / ethanol; dimethyl sulfoxide

With dihydrogen peroxide; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; potassium hydroxide; In 1,4-dioxane; ethanol; dimethyl sulfoxide; 1: Buchwald amination;
DOI:10.1016/j.bmcl.2011.09.090