(8S,9S,10R,13R,14S,17R)-3-[1-Benzenesulfinyl-meth-(Z)-ylidene]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Base Information

• Chemical Name: (8S,9S,10R,13R,14S,17R)-3-[1-Benzenesulfinyl-meth-(Z)-ylidene]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene
• CAS No.: 66967-46-2
• Molecular Formula: C₃₄H₅₀OS
• Molecular Weight: 506.836

Synonyms:

Chemical Property of (8S,9S,10R,13R,14S,17R)-3-[1-Benzenesulfinyl-meth-(Z)-ylidene]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of (8S,9S,10R,13R,14S,17R)-3-[1-Benzenesulfinyl-meth-(Z)-ylidene]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

There total 1 articles about (8S,9S,10R,13R,14S,17R)-3-[1-Benzenesulfinyl-meth-(Z)-ylidene]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C11H16LiO3PS + (8S,9S,10R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-cyclopenta[a]phenanthren-3-one (601-57-0,14615-14-6,23820-66-8,38777-61-6) → (8S,9S,10R,13R,14S,17R)-3-[1-Benzenesulfinyl-meth-(Z)-ylidene]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene (66967-46-2,66967-54-2)

Guidance literature:

In tetrahydrofuran;

DOI:10.1021/jo00415a032

Reference yield:

(8S,9S,10R,13R,14S,17R)-3-[1-Benzenesulfinyl-meth-(Z)-ylidene]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene (66967-46-2,66967-54-2) → (8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-3-[1-phenylsulfanyl-meth-(Z)-ylidene]-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene (66967-53-1,66967-55-3)

Guidance literature:

With copper(l) iodide; ethylmagnesium bromide; In diethyl ether;

DOI:10.1021/jo00415a032

upstream raw materials:

(8S,9S,10R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-cyclopenta[a]phenanthren-3-one

Downstream raw materials:

(8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-3-[1-phenylsulfanyl-meth-(Z)-ylidene]-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

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