1,5-Diamino-3-methylpentane

Base Information

• Chemical Name: 1,5-Diamino-3-methylpentane
• CAS No.: 123952-70-5
• Molecular Formula: C6H16N2
• Molecular Weight: 116.20500
• Mol file: 123952-70-5.mol

Synonyms:1,5-Diamino-3-methylpentane;3-methyl-1,5-diaminopentane;1,5-Diamino-3-methyl-pentan;3-methylcadaverine;1,5-Pentanediamine,3-methyl;

Chemical Property of 1,5-Diamino-3-methylpentane

Chemical Property:

• PSA: 52.04000
• LogP: 1.72070

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,5-Diamino-3-methylpentane

There total 8 articles about 1,5-Diamino-3-methylpentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3-methyl-(1,5)-azopentane → 1,5-Diamino-3-methylpentane (123952-70-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1016/j.tet.2008.05.021

Reference yield:

β-Methylglutaronitrile (32091-48-8) → 1,5-Diamino-3-methylpentane (123952-70-5)

Guidance literature:

With ammonia; hydrogen; Raney-Co; at 120 - 140 ℃; under 73550.8 Torr;

Reference yield:

3-methylpentane-1,5-diol (4457-71-0) → 1,5-Diamino-3-methylpentane (123952-70-5)

Guidance literature:

With hydrogen azide; triphenylphosphine; 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; benzene; Yield given; 1) 1h, RT, 2) 50 deg C, 3h;

DOI:10.1016/S0040-4020(01)90506-X

upstream raw materials:

β-Methylglutaronitrile

3-methylpentane-1,5-diol

3-methyl glutaric acid

3-methyl-pentenedinitrile

Downstream raw materials:

N,N'-(3-methylpentane-1,5-diyl)bis(2,3-dimethoxybenzamide)

C₂₀H₂₄N₂O₆

2-(4-Methyl-piperidin-2-yl)-1-phenyl-ethanone

Refernces

• 1、 Yang, Donglai,Arifhodzic, Lejla,Ganellin, C. Robin,Jenkinson, Donald H.. "Further studies on bis-charged tetraazacyclophanes as potent inhibitors of small conductance Ca2+-activated K+ channels". supporting information. p. 907 - 923. Retrieved 2013/07/27.
• 2、 -. "Potent inducers of terminal differentiation and methods of use thereof". . . Retrieved 2008/06/13.