Technology Process of C12H11IO5
There total 4 articles about C12H11IO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfuric acid / water / 1 h / Cooling with ice
2: Iodine monochloride / chloroform / 1 h / Reflux
3: water / 1.5 h / Reflux; Cooling with ice
With
sulfuric acid; water; Iodine monochloride;
In
chloroform; water;
DOI:10.1007/s00044-010-9394-2
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Iodine monochloride / chloroform / 1 h / Reflux
2: water / 1.5 h / Reflux; Cooling with ice
With
water; Iodine monochloride;
In
chloroform;
DOI:10.1007/s00044-010-9394-2
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / ethanol; water / 8 - 20 °C
2: sulfuric acid / water / 1 h / Cooling with ice
3: Iodine monochloride / chloroform / 1 h / Reflux
4: water / 1.5 h / Reflux; Cooling with ice
With
sulfuric acid; water; Iodine monochloride; sodium hydroxide;
In
ethanol; chloroform; water;
DOI:10.1007/s00044-010-9394-2