C₅₁H₆₄N₈O₁₁S

Base Information

Chemical Name:C₅₁H₆₄N₈O₁₁S
CAS No.:1389332-37-9
Molecular Formula:C₅₁H₆₄N₈O₁₁S
Molecular Weight:997.182
Hs Code.:

C<sub>51</sub>H<sub>64</sub>N<sub>8</sub>O<sub>11</sub>S

Synonyms:

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Chemical Property of C₅₁H₆₄N₈O₁₁S

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Technology Process of C₅₁H₆₄N₈O₁₁S

There total 6 articles about C₅₁H₆₄N₈O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂HF₃O₂*C₁₆H₂₁N₅O₅

: 1389332-37-9
C₅₁H₆₄N₈O₁₁S

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 5 h / 20 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

2.2: 3 h / -40 °C / Inert atmosphere

3.1: trimethylphosphane / tetrahydrofuran; toluene / 6 h / -20 - 20 °C / Inert atmosphere

4.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

5.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

With 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine; HATU; trimethylphosphane; In tetrahydrofuran; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene;
DOI:10.1002/chem.201200457

Reference yield:

: 1389332-02-8
C₂₁H₂₉N₅O₇

: 1389332-37-9
C₅₁H₆₄N₈O₁₁S

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylsilane / dichloromethane / 2 h / 20 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 5 h / 20 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

3.2: 3 h / -40 °C / Inert atmosphere

4.1: trimethylphosphane / tetrahydrofuran; toluene / 6 h / -20 - 20 °C / Inert atmosphere

5.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

6.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

6.2: 0 - 20 °C / Inert atmosphere

With triethylsilane; 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine; HATU; trimethylphosphane; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene;
DOI:10.1002/chem.201200457

Reference yield:

: 1389332-03-9
C₁₅H₁₇N₅O₄

: 1389332-37-9
C₅₁H₆₄N₈O₁₁S

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

1.2: 3 h / -40 °C / Inert atmosphere

2.1: trimethylphosphane / tetrahydrofuran; toluene / 6 h / -20 - 20 °C / Inert atmosphere

3.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

4.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

4.2: 0 - 20 °C / Inert atmosphere

With 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine; HATU; trimethylphosphane; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene;
DOI:10.1002/chem.201200457