1-(4-Chloro-phenyl)-2-methyl-but-3-en-1-ol

Base Information

Chemical Name:1-(4-Chloro-phenyl)-2-methyl-but-3-en-1-ol
CAS No.:123989-31-1
Molecular Formula:C11H13ClO
Molecular Weight:196.677
Hs Code.:
European Community (EC) Number:602-965-9
DSSTox Substance ID:DTXSID701010223
Nikkaji Number:J1.034.013F
Mol file:123989-31-1.mol

Synonyms:1-(4-chloro-phenyl)-2-methyl-but-3-en-1-ol;123989-31-1;EC 602-965-9;1-(4-chlorophenyl)-2-methylbut-3-en-1-ol;3-methyl-4-(4-chlorophenyl)-but-1-en-4-ol;SCHEMBL8649655;UUZUQJOJASRJBK-UHFFFAOYSA-N;DTXSID701010223;1-(4-chlorophenyl)-2-methyl-3-buten-1-ol;3-Methyl-4-(4-chlorophenyl)but-1-en-4-ol;NS00003957

Suppliers and Price of 1-(4-Chloro-phenyl)-2-methyl-but-3-en-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-(4-Chloro-phenyl)-2-methyl-but-3-en-1-ol

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:196.0654927
Heavy Atom Count:13
Complexity:162

Purity/Quality:: 99.9% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C=C)C(C1=CC=C(C=C1)Cl)O

Technology Process of 1-(4-Chloro-phenyl)-2-methyl-but-3-en-1-ol

There total 35 articles about 1-(4-Chloro-phenyl)-2-methyl-but-3-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 104-88-1
4-chlorobenzaldehyde

: 69611-01-4
(Z)-2-(but-2-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 123989-31-1,128624-10-2,128624-11-3
(±)-syn-1-(4-chlorophenyl)-2-methylbut-3-en-1-ol

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; nickel(II) acetate tetrahydrate; In tetrahydrofuran; at 20 ℃; for 18h; diastereoselective reaction; Inert atmosphere;
DOI:10.1055/s-0039-1690091

Reference yield: 98.0%

: 104-88-1
4-chlorobenzaldehyde

: 2-(but-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 123989-31-1,128624-10-2,128624-11-3
(±)-syn-1-(4-chlorophenyl)-2-methylbut-3-en-1-ol

Guidance literature:: With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); diphenylphosphane; zinc(II) iodide; zinc; In dichloromethane; at -40 ℃; for 1h; diastereoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.5b03585