4-(acetylamino)-5-acetoxy-1,3-dihydro-1-(p-tolylsulfonyl)benzindole

Base Information

Chemical Name:4-(acetylamino)-5-acetoxy-1,3-dihydro-1-(p-tolylsulfonyl)benzindole
CAS No.:81206-39-5
Molecular Formula:C₂₂H₂₀N₂O₅S
Molecular Weight:424.477
Hs Code.:

4-(acetylamino)-5-acetoxy-1,3-dihydro-1-(p-tolylsulfonyl)benz<cd>indole

Synonyms:

Suppliers and Price of 4-(acetylamino)-5-acetoxy-1,3-dihydro-1-(p-tolylsulfonyl)benzindole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(acetylamino)-5-acetoxy-1,3-dihydro-1-(p-tolylsulfonyl)benzindole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(acetylamino)-5-acetoxy-1,3-dihydro-1-(p-tolylsulfonyl)benzindole

There total 1 articles about 4-(acetylamino)-5-acetoxy-1,3-dihydro-1-(p-tolylsulfonyl)benzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81206-38-4
4-azido-1-(toluene-4-sulfonyl)-3,4-dihydro-1H-benzo[c,d]indol-5-one

: 108-24-7
acetic anhydride

: 81206-39-5
4-(acetylamino)-5-acetoxy-1,3-dihydro-1-(p-tolylsulfonyl)benzindole

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 2h; Ambient temperature;
DOI:10.1021/jo00132a040

Reference yield:

: 81206-39-5
4-(acetylamino)-5-acetoxy-1,3-dihydro-1-(p-tolylsulfonyl)benzindole

: 81218-97-5
trans-4-(acetylamino)-1,3,4,5-tetrahydro-1-(p-tolylsulfonyl)benzindol-5-ol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; ethanol; for 1h; Ambient temperature;
DOI:10.1021/jo00132a040

Reference yield:

: 81206-39-5
4-(acetylamino)-5-acetoxy-1,3-dihydro-1-(p-tolylsulfonyl)benzindole

: 81244-90-8
(-)-trans-4-(acetylamino)-1,3,4,5-tetrahydro-1-(p-tolylsulfonyl)benzindol-5-ol

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / tetrahydrofuran; ethanol / 1 h / Ambient temperature

2: dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 1.5 h

3: 100 percent / KOH / ethanol / 0.17 h / 50 - 55 °C

With dmap; potassium hydroxide; sodium tetrahydroborate; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jo00132a040