C₂₁H₂₁N₃O₂S₃

Base Information

Chemical Name:C₂₁H₂₁N₃O₂S₃
CAS No.:1297473-48-3
Molecular Formula:C₂₁H₂₁N₃O₂S₃
Molecular Weight:443.615
Hs Code.:

C<sub>21</sub>H<sub>21</sub>N<sub>3</sub>O<sub>2</sub>S<sub>3</sub>

Synonyms:

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Chemical Property of C₂₁H₂₁N₃O₂S₃

Chemical Property:

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Technology Process of C₂₁H₂₁N₃O₂S₃

There total 4 articles about C₂₁H₂₁N₃O₂S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7442-07-1
6-amino-2-mercaptobenzothiazole

: 1297473-48-3
C₂₁H₂₁N₃O₂S₃

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / 16 h / 50 °C

2: triethylamine / 8 h / 20 °C / Inert atmosphere

3: triethylamine / N,N-dimethyl-formamide / 16 h / 50 °C

With triethylamine; In N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201000507

Reference yield:

: 312285-34-0
C₁₂H₁₃N₃OS₂

: 1297473-48-3
C₂₁H₂₁N₃O₂S₃

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 8 h / 20 °C / Inert atmosphere

2: triethylamine / N,N-dimethyl-formamide / 16 h / 50 °C

With triethylamine; In N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201000507

Reference yield:

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 1297473-48-3
C₂₁H₂₁N₃O₂S₃

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; nitric acid / 2 h / 0 °C / Inert atmosphere

2: sodium sulfide; sodium hydrogen sulfide; sulfur / water / 24 h / Reflux; Inert atmosphere

3: triethylamine / 16 h / 50 °C

4: triethylamine / 8 h / 20 °C / Inert atmosphere

5: triethylamine / N,N-dimethyl-formamide / 16 h / 50 °C

With sodium hydrogen sulfide; sodium sulfide; sulfuric acid; nitric acid; sulfur; triethylamine; In water; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201000507