C₅₀H₈₈O₁₀Si₂

Base Information

• Chemical Name: C₅₀H₈₈O₁₀Si₂
• CAS No.: 1418006-31-1
• Molecular Formula: C₅₀H₈₈O₁₀Si₂
• Molecular Weight: 905.414
• Mol file: 1418006-31-1.mol

Synonyms:

Chemical Property of C₅₀H₈₈O₁₀Si₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₀H₈₈O₁₀Si₂

There total 4 articles about C₅₀H₈₈O₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

C16H34O2Si (1227185-11-6) + C34H54O8Si (1417998-35-6) → C50H88O10Si2 (1418006-31-1)

Guidance literature:

With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; Reagent/catalyst; Inert atmosphere;

DOI:10.1246/bcsj.20120162

Reference yield:

(S)-2-methylbutyraldehyde (1730-97-8) → C50H88O10Si2 (1418006-31-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.67 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 1.25 h / 20 °C / Inert atmosphere

3.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere

With 1H-imidazole; sodium hexamethyldisilazane; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1246/bcsj.20120162

Reference yield:

(2S)-2-methyl-1-butanol (1565-80-6) → C50H88O10Si2 (1418006-31-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: oxalyl dichloride; N-ethyl-N,N-diisopropylamine; dimethyl sulfoxide / dichloromethane / -78 - 0 °C / Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.67 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

3.1: 1H-imidazole / N,N-dimethyl-formamide / 1.25 h / 20 °C / Inert atmosphere

4.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere

With 1H-imidazole; oxalyl dichloride; sodium hexamethyldisilazane; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1246/bcsj.20120162

upstream raw materials:

(S)-2-methylbutyraldehyde

(2S)-2-methyl-1-butanol

C₁₆H₃₄O₂Si

C₃₄H₅₄O₈Si