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(20ξ)-5α-Dammara-24-ene-3β,20-diol

Base Information Edit
  • Chemical Name:(20ξ)-5α-Dammara-24-ene-3β,20-diol
  • CAS No.:19132-83-3
  • Molecular Formula:C30H52O2
  • Molecular Weight:444.742
  • Hs Code.:
  • Mol file:19132-83-3.mol
(20ξ)-5α-Dammara-24-ene-3β,20-diol

Synonyms:

Suppliers and Price of (20ξ)-5α-Dammara-24-ene-3β,20-diol
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
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Total 3 raw suppliers
Chemical Property of (20ξ)-5α-Dammara-24-ene-3β,20-diol Edit
Chemical Property:
Purity/Quality:

99% *data from raw suppliers

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Technology Process of (20ξ)-5α-Dammara-24-ene-3β,20-diol

There total 74 articles about (20ξ)-5α-Dammara-24-ene-3β,20-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 28 steps
1: Et3N / 1,2-dimethoxy-ethane / 23 °C
2: (S)-phenylalanine, (+)-camphorsulfonic acid / dimethylformamide / 576 h / 23 °C
3: 1.) potassium hexamethyldisilazide, Et3B / 1.) THF, -78 deg C, 2.) -25 deg C, 2 h
4: HgCl2, water, pyridine / tetrahydrofuran / 36 h / 23 °C
5: Cs2CO3 / tetrahydrofuran / 16 h / 23 °C
6: 77 percent / lithium trisiamylborohydride / tetrahydrofuran / -40 °C
7: 1.) n-BuLi / 1.) ether, -20 deg C, 2.) 23 deg C, 12 h
8: 94 percent / C6H5NMe2 / 1 h / 20 °C
9: 1.) Li, liquid NH3, water / 1.) THF, -40 deg C, 3 min, 2.) -70 deg C, 1 h
10: 0.02percent aq. HCl / acetone / 20 h / 23 °C
11: 1percent aq. KOH / methanol / 6 h / Heating
12: 100 percent / sodium borohydride / tetrahydrofuran; methanol / 1 h / 0 °C
14: 97 percent / methylmagnesium isopropylcyclohexylamide / diethyl ether; toluene / 12 h / 4 °C
15: periodinane / CH2Cl2 / 1 h / 23 °C
16: 1.) Li, liquid NH3, water / 1.) THF, -40 deg C, 3 min, 2.) 30 min
17: 95 percent / NaBH4 / tetrahydrofuran; methanol / 0 °C
18: 98 percent / imidazole / dimethylformamide / 12 h / 50 °C
19: 94 percent / diphenylbromoborane / CH2Cl2 / 0.17 h / -40 °C
20: 95 percent / pyridinium chlorochromate on Al2O3 / CH2Cl2 / 5 h / 23 °C
22: 92 percent / Li, liquid NH3, water / tetrahydrofuran / 0.67 h / -50 °C
23: 1.) n-BuLi / 1.) THF, -20 deg C, 2.) 23 deg C, 2 h
24: Li, EtNH2 / 2-methyl-propan-2-ol / 0.5 h / 0 °C
25: 95 percent / 1percent CF3CO2H / tetrahydrofuran; H2O / 3 h / 23 °C
26: 93 percent / pyridinium chlorochromate on Al2O3 / CH2Cl2 / 5 h / 20 °C
27: 30 percent / diethyl ether / 0.5 h / 0 °C
28: 100 percent / Bu4NF / tetrahydrofuran / 10 h / 50 °C
With pyridine; 1H-imidazole; hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; n-butyllithium; triethyl borane; L-phenylalanine; pyridiniumchlorochromate on aluminumoxide; bromodiphenylborane; tetrabutyl ammonium fluoride; ammonia; water; lithium; potassium hexamethylsilazane; methylmagnesium N-cyclohexylisopropylamide; caesium carbonate; Dess-Martin periodane; ethylamine; N,N-dimethyl-aniline; (+)-10-camphorsulfonic acid; lithium tri-sec-butyl(hydrido)borate; triethylamine; trifluoroacetic acid; mercury dichloride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol;
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