Technology Process of C22H24N2O7
There total 5 articles about C22H24N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
1,4-dioxane;
at 20 ℃;
for 24h;
DOI:10.1016/j.bmcl.2012.10.122
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene-4-sulfonic acid / 24 h / Reflux
2: potassium permanganate / water; acetone / 24 h / -10 - 20 °C
3: sodium acetate; acetic anhydride / 3 h / Reflux
4: sodium tetrahydroborate / methanol / 2 h / 20 °C
5: di-isopropyl azodicarboxylate; triphenylphosphine / 1,4-dioxane / 24 h / 20 °C
With
sodium tetrahydroborate; potassium permanganate; di-isopropyl azodicarboxylate; sodium acetate; acetic anhydride; toluene-4-sulfonic acid; triphenylphosphine;
In
1,4-dioxane; methanol; water; acetone;
3: |Dieckmann Condensation / 5: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2012.10.122
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium acetate; acetic anhydride / 3 h / Reflux
2: sodium tetrahydroborate / methanol / 2 h / 20 °C
3: di-isopropyl azodicarboxylate; triphenylphosphine / 1,4-dioxane / 24 h / 20 °C
With
sodium tetrahydroborate; di-isopropyl azodicarboxylate; sodium acetate; acetic anhydride; triphenylphosphine;
In
1,4-dioxane; methanol;
1: |Dieckmann Condensation / 3: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2012.10.122
