N-<(3S)-3-<(3S)-3-Benzyloxycarbonylamino-3-tert.-butyloxycarbonylpropylamino>-3-tert.-butyloxycarbonylpropyl>-N-tert.-butyloxycarbonyl-glycin-tert.-butylester

Base Information

Chemical Name:N-<(3S)-3-<(3S)-3-Benzyloxycarbonylamino-3-tert.-butyloxycarbonylpropylamino>-3-tert.-butyloxycarbonylpropyl>-N-tert.-butyloxycarbonyl-glycin-tert.-butylester
CAS No.:125786-12-1
Molecular Formula:C₃₅H₅₇N₃O₁₀
Molecular Weight:679.852
Hs Code.:

N-<(3S)-3-<(3S)-3-Benzyloxycarbonylamino-3-tert.-butyloxycarbonylpropylamino>-3-tert.-butyloxycarbonylpropyl>-N-tert.-butyloxycarbonyl-glycin-tert.-butylester

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Chemical Property of N-<(3S)-3-<(3S)-3-Benzyloxycarbonylamino-3-tert.-butyloxycarbonylpropylamino>-3-tert.-butyloxycarbonylpropyl>-N-tert.-butyloxycarbonyl-glycin-tert.-butylester

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Technology Process of N-<(3S)-3-<(3S)-3-Benzyloxycarbonylamino-3-tert.-butyloxycarbonylpropylamino>-3-tert.-butyloxycarbonylpropyl>-N-tert.-butyloxycarbonyl-glycin-tert.-butylester

There total 6 articles about N-<(3S)-3-<(3S)-3-Benzyloxycarbonylamino-3-tert.-butyloxycarbonylpropylamino>-3-tert.-butyloxycarbonylpropyl>-N-tert.-butyloxycarbonyl-glycin-tert.-butylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 78553-60-3
1,1-dimethylethyl (S)-4-oxo-2-[[(phenylmethoxy)-carbonyl]amino]butanoate

: 125786-10-9
N-<(3S)-3-Amino-3-tert.-butyloxycarbonylpropyl>-N-tert.-butyloxycarbonyl-glycin-tert.-butylester

: 125786-12-1
N-<(3S)-3-<(3S)-3-Benzyloxycarbonylamino-3-tert.-butyloxycarbonylpropylamino>-3-tert.-butyloxycarbonylpropyl>-N-tert.-butyloxycarbonyl-glycin-tert.-butylester

Guidance literature:: With sodium cyanoborohydride; In methanol; for 24h; Ambient temperature;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 125786-12-1
N-<(3S)-3-<(3S)-3-Benzyloxycarbonylamino-3-tert.-butyloxycarbonylpropylamino>-3-tert.-butyloxycarbonylpropyl>-N-tert.-butyloxycarbonyl-glycin-tert.-butylester

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / triethylamine / CH₂Cl₂ / 20 h / Ambient temperature

2: 88 percent / H₂ / 10percent Pd/C / propan-2-ol / Ambient temperature

3: 66 percent / NaBH₃CN / methanol / 24 h / Ambient temperature

With hydrogen; sodium cyanoborohydride; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; isopropyl alcohol;

Reference yield:

: 6456-74-2
Glycine tert-butyl ester

: 125786-12-1
N-<(3S)-3-<(3S)-3-Benzyloxycarbonylamino-3-tert.-butyloxycarbonylpropylamino>-3-tert.-butyloxycarbonylpropyl>-N-tert.-butyloxycarbonyl-glycin-tert.-butylester

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / NaBH₃CN / methanol / 24 h / Ambient temperature

2: 76 percent / triethylamine / CH₂Cl₂ / 20 h / Ambient temperature

3: 88 percent / H₂ / 10percent Pd/C / propan-2-ol / Ambient temperature

4: 66 percent / NaBH₃CN / methanol / 24 h / Ambient temperature

With hydrogen; sodium cyanoborohydride; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; isopropyl alcohol;