(S)-1-tosyl-3-morpholinopyrrolidine

Base Information

Chemical Name:(S)-1-tosyl-3-morpholinopyrrolidine
CAS No.:216669-62-4
Molecular Formula:C₁₅H₂₂N₂O₃S
Molecular Weight:310.417
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-tosyl-3-morpholinopyrrolidine

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Technology Process of (S)-1-tosyl-3-morpholinopyrrolidine

There total 2 articles about (S)-1-tosyl-3-morpholinopyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 110-91-8,99108-56-2
morpholine

: (R)-toluene-4-sulfonic acid 1-(toluene-4-sulfonyl)-pyrrolidin-3-yl ester

: 216669-62-4
(S)-1-tosyl-3-morpholinopyrrolidine

Guidance literature:: at 85 ℃; for 6h;
DOI:10.1021/jo9810260

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 216669-62-4
(S)-1-tosyl-3-morpholinopyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / pyridine; DMAP / CH₂Cl₂ / 48 h / 0 - 20 °C

2: 90 percent / 6 h / 85 °C

With pyridine; dmap; In dichloromethane; 1: Tosylation / 2: Substitution;
DOI:10.1021/jo9810260