Technology Process of C26H38F2N2OSn
There total 5 articles about C26H38F2N2OSn which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium diisopropyl amide;
In
tetrahydrofuran; cyclohexane;
at -78 - 20 ℃;
for 3h;
DOI:10.1021/jm401621g
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: boron tribromide / dichloromethane / 2.5 h / -20 °C
1.2: 20 °C / pH 7
2.1: sodium hydroxide / water; isopropyl alcohol / 2 h / 75 °C
3.1: lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 3 h / -78 - 20 °C
With
boron tribromide; sodium hydroxide; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; cyclohexane; water; isopropyl alcohol;
DOI:10.1021/jm401621g
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N,N-dimethyl-formamide / 1.5 h / -20 - -10 °C / Cooling with acetone-dry ice
2.1: caesium carbonate / N,N-dimethyl-formamide / 100 °C
3.1: boron tribromide / dichloromethane / 2.5 h / -20 °C
3.2: 20 °C / pH 7
4.1: sodium hydroxide / water; isopropyl alcohol / 2 h / 75 °C
5.1: lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 3 h / -78 - 20 °C
With
boron tribromide; caesium carbonate; sodium hydroxide; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm401621g