(+/-)-cis-4'-hydroxy-γ-ionone

Base Information

Chemical Name:(+/-)-cis-4'-hydroxy-γ-ionone
CAS No.:38963-37-0
Molecular Formula:C₁₃H₂₂O₂
Molecular Weight:210.316
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-cis-4'-hydroxy-γ-ionone

Chemical Property:

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Technology Process of (+/-)-cis-4'-hydroxy-γ-ionone

There total 13 articles about (+/-)-cis-4'-hydroxy-γ-ionone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (+/-)-4'-Tetrahydropyranyloxy-γ-ionone

: 38963-37-0
(+/-)-cis-4'-hydroxy-γ-ionone

Guidance literature:: With acetic acid; In tetrahydrofuran; for 24h; Ambient temperature; H₂O-AcOH-THF = 1:2:1;

Reference yield:

: (+/-)-1-Chloromethyl-3,3-dimethyl-5-tetrahydropyranyloxy-1-cyclohexene

: 38963-37-0
(+/-)-cis-4'-hydroxy-γ-ionone

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / K₂CO₃ / dimethylformamide / 24 h / 70 °C

2: 74 percent / toluene / 20 h / Heating

3: aqueous acetic acid / tetrahydrofuran / 24 h / Ambient temperature; H₂O-AcOH-THF = 1:2:1

With potassium carbonate; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

Reference yield:

: (+/-)-2,2-Dimethyl-4-tetrahydropyranyloxy-1-cyclohexanone

: 38963-37-0
(+/-)-cis-4'-hydroxy-γ-ionone

Guidance literature:: Multi-step reaction with 8 steps

1: MeONa

2: 85 percent / 85percent H₃PO₄ / CH₂Cl₂ / 6 h / 20 °C

3: 82 percent / NaBH₄ / ethanol / 1 h

4: LiAlH₄ / diethyl ether / 1 h

5: Chlorodimethylformimium chlorid / dimethylformamide / 1 h

6: 75 percent / K₂CO₃ / dimethylformamide / 24 h / 70 °C

7: 74 percent / toluene / 20 h / Heating

8: aqueous acetic acid / tetrahydrofuran / 24 h / Ambient temperature; H₂O-AcOH-THF = 1:2:1

With sodium tetrahydroborate; lithium aluminium tetrahydride; phosphoric acid; Vilsmeier reagent; sodium methylate; potassium carbonate; acetic acid; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;