3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetracyclohexyl ester

Base Information

Chemical Name:3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetracyclohexyl ester
CAS No.:124686-88-0
Molecular Formula:C₄₈H₆₆MnO₁₂PS
Molecular Weight:953.023
Hs Code.:

3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetracyclohexyl ester

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Chemical Property of 3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetracyclohexyl ester

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Technology Process of 3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetracyclohexyl ester

There total 1 articles about 3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetracyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 119208-87-6
Tetracarbonyl(η2-dicyclohexylthiophosphinito)mangan(I)

: 79866-97-0
acetylenedicarboxylic acid dicyclohexyl ester

: 124686-88-0
3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetracyclohexyl ester

Guidance literature:: In hexane; addn. of alkine to soln. of Mn-complex, stirring 12h (Ar); pptn., filtration, washing (hexane), medium pressure column chromy. (silica gel, CH2Cl2-EtOAc); elem. anal.;

Reference yield: 95.0%

: 124686-88-0
3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetracyclohexyl ester

: 124686-95-9
7,7,7-tricarbonyl-3,3-dicyclohexyl-2λ(3)-thia-3λ(5)-phospha-η2-7-manganabicyclo{2.2.1}hepta-2,5-diene-1,4,5,6-tetracarboxylic acid tetracyclohexyl ester

Guidance literature:: In toluene; byproducts: CO; stirring soln. of educt 4h at 80°C with occasional vacuum (Ar); evapn. (vacuum), column chromy. (silica gel, CH2Cl2-EtOAc); elem. anal.;