Technology Process of (4S,7R)-3,3-Dimethyl-1,6-dioxo-7-phenylacetylamino-1λ4-[1,2,5]dithiazocane-4-carboxylic acid methyl ester
There total 4 articles about (4S,7R)-3,3-Dimethyl-1,6-dioxo-7-phenylacetylamino-1λ4-[1,2,5]dithiazocane-4-carboxylic acid methyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) triethylamine, EEDQ, 2.) aqueous 5M-HCl, Zn dust / 1.) tetrahydrofuran, room temperature, 25 h, 2.) MeOH, 0 deg C, 30 min
2: 0.60 g / iodine / methanol / 2 h / Heating
3: 100 mg / 3-chloroperbenzoic acid / CHCl3 / 18 h / Ambient temperature
With
hydrogenchloride; iodine; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; 3-chloro-benzenecarboperoxoic acid; zinc;
In
methanol; chloroform;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) triethylamine, EEDQ, 2.) aqueous 5M-HCl, Zn dust / 1.) tetrahydrofuran, room temperature, 25 h, 2.) MeOH, 0 deg C, 30 min
2: 0.60 g / iodine / methanol / 2 h / Heating
3: 100 mg / 3-chloroperbenzoic acid / CHCl3 / 18 h / Ambient temperature
With
hydrogenchloride; iodine; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; 3-chloro-benzenecarboperoxoic acid; zinc;
In
methanol; chloroform;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 0.60 g / iodine / methanol / 2 h / Heating
2: 100 mg / 3-chloroperbenzoic acid / CHCl3 / 18 h / Ambient temperature
With
iodine; 3-chloro-benzenecarboperoxoic acid;
In
methanol; chloroform;
