C₂₅H₂₈N₂O₂

Base Information

Chemical Name:C₂₅H₂₈N₂O₂
CAS No.:1416772-63-8
Molecular Formula:C₂₅H₂₈N₂O₂
Molecular Weight:388.51
Hs Code.:

C<sub>25</sub>H<sub>28</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₅H₂₈N₂O₂

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Technology Process of C₂₅H₂₈N₂O₂

There total 11 articles about C₂₅H₂₈N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416772-62-7
C₂₆H₃₂N₂O₃

: 1416772-63-8
C₂₅H₂₈N₂O₂

Guidance literature:: With sodium periodate; In dichloromethane; water; at 20 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ml300385q

Reference yield:

: 1416772-52-5
C₂₆H₃₀N₂O

: 1416772-63-8
C₂₅H₂₈N₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1: AD-mix-α; methanesulfonamide / water; tert-butyl alcohol / 72 h / 20 °C / Inert atmosphere; Schlenk technique

2: sodium periodate / dichloromethane; water / 2 h / 20 °C / Inert atmosphere; Schlenk technique

With sodium periodate; methanesulfonamide; AD-mix-α; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ml300385q

Reference yield:

: 89890-92-6
N-acetyl-(β-3-pyridyl)-α,β-dehydroalanine

: 1416772-63-8
C₂₅H₂₈N₂O₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium acetate / 72 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: tetrafluoroboric acid; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / methanol / 18 h / 50 °C / 3750.38 Torr / Autoclave; Schlenk technique

3.1: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

4.1: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

5.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

6.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

7.1: chromium dichloride / tetrahydrofuran / 0.42 h / 200 °C / Inert atmosphere; Schlenk technique

7.2: 3 h / 20 °C

8.1: AD-mix-α; methanesulfonamide / water; tert-butyl alcohol / 72 h / 20 °C / Inert atmosphere; Schlenk technique

9.1: sodium periodate / dichloromethane; water / 2 h / 20 °C / Inert atmosphere; Schlenk technique

With chromium dichloride; sodium periodate; lithium aluminium tetrahydride; tetrafluoroboric acid; thionyl chloride; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; methanesulfonamide; AD-mix-α; hydrogen; sodium acetate; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ml300385q