IrCl(CO){Ph2P(η5-C5H4)Ir(CO)(PPh3)}2

Base Information

Chemical Name:IrCl(CO){Ph2P(η5-C5H4)Ir(CO)(PPh3)}2
CAS No.:106520-03-0
Molecular Formula:C₇₃H₅₈ClIr₃O₃P₄
Molecular Weight:1719.27
Hs Code.:

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Chemical Property of IrCl(CO){Ph2P(η5-C5H4)Ir(CO)(PPh3)}2

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Technology Process of IrCl(CO){Ph2P(η5-C5H4)Ir(CO)(PPh3)}2

There total 2 articles about IrCl(CO){Ph2P(η5-C5H4)Ir(CO)(PPh3)}2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 83272-80-4
lithium diphenylphosphinocyclopentadienyl

: 106500-77-0
Ph2P(η5-C5H4)Ir(CO)(PPh3)

: 106500-78-1
{Ph2P(η5-C5H4)Ir(CO)}2

: 106520-03-0
IrCl(CO){Ph2P(η5-C5H4)Ir(CO)(PPh3)}2

Guidance literature:: In toluene; byproducts: P(C6H5)3, LiCl; addn. of Li(C5H4)PPh2 to trans-IrCl(CO)(PPh3)2 (Ir/LiCpP molar ratio ca. 1:1) in toluene at 70°C, react. time 5 min; Ir2 species formed yellow ppt.; elem. anal.;

Reference yield: 10.0%

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 83272-80-4
lithium diphenylphosphinocyclopentadienyl

: 106500-78-1
{Ph2P(η5-C5H4)Ir(CO)}2

: 106520-03-0
IrCl(CO){Ph2P(η5-C5H4)Ir(CO)(PPh3)}2

Guidance literature:: In toluene; react. mixt. (N2 or Ar, slight excess of trans-IrCl(CO)(PPh3)2, room temp.), orange soln., heated (70 °C., 1 h); ppt. sepd. (= (Ph2P(C5H4)Ir(CO)2); pentane added to the filtrate, yellow ppt. decanted, washed (petroleum ether), dried (vac.), comp. = (IrCl(CO)Ph2P(C5H4)Ir(CO)(PPh3))2, elem. anal.;