Benzoic acid, 2-iodo-3,5-dimethoxy-

Base Information

Chemical Name:Benzoic acid, 2-iodo-3,5-dimethoxy-
CAS No.:124481-00-1
Molecular Formula:C9H9IO4
Molecular Weight:308.073
Hs Code.:
DSSTox Substance ID:DTXSID40458122
Nikkaji Number:J1.793.345K
Wikidata:Q82281272
Mol file:124481-00-1.mol

Synonyms:Benzoic acid, 2-iodo-3,5-dimethoxy-;2-Iodo-3,5-dimethoxybenzoic acid;124481-00-1;DTXSID40458122

Suppliers and Price of Benzoic acid, 2-iodo-3,5-dimethoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzoic acid, 2-iodo-3,5-dimethoxy-

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:307.95456
Heavy Atom Count:14
Complexity:209

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C(=C1)OC)I)C(=O)O

Technology Process of Benzoic acid, 2-iodo-3,5-dimethoxy-

There total 4 articles about Benzoic acid, 2-iodo-3,5-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 114605-46-8
methyl 2-iodo-3,5-dimethoxybenzoate

: 124481-00-1
2-iodo-3,5-dimethoxybenzoic acid

Guidance literature:: With sodium hydroxide; In methanol; ethanol; at 70 - 80 ℃; for 1h;
DOI:10.1021/ol026182e

Reference yield:

: 99-10-5
3,5-Dihydroxybenzoic acid

: 124481-00-1
2-iodo-3,5-dimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / NaOH

2: 87 percent / HNO₃, acetic anhydride / acetic acid

3: 69 percent / FeSO₄, NH₃

4: 1.) aq. NaNO₃, concd. H₂SO₄, 2.) aq. KI / 1.) water, 0 deg C, 2.) reflux, 30 min

With sodium hydroxide; sodium nitrate; sulfuric acid; ammonia; nitric acid; acetic anhydride; iron(II) sulfate; potassium iodide; In acetic acid;

Reference yield:

: 1132-21-4
3,5-dimethoxybenzoic acid

: 124481-00-1
2-iodo-3,5-dimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / HNO₃, acetic anhydride / acetic acid

2: 69 percent / FeSO₄, NH₃

3: 1.) aq. NaNO₃, concd. H₂SO₄, 2.) aq. KI / 1.) water, 0 deg C, 2.) reflux, 30 min

With sodium nitrate; sulfuric acid; ammonia; nitric acid; acetic anhydride; iron(II) sulfate; potassium iodide; In acetic acid;