p-cyanophenylchlorocarbene

Base Information

Chemical Name:p-cyanophenylchlorocarbene
CAS No.:882528-49-6
Molecular Formula:C₈H₄ClN
Molecular Weight:149.579
Hs Code.:

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Suppliers and Price of p-cyanophenylchlorocarbene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-cyanophenylchlorocarbene

Chemical Property:

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Technology Process of p-cyanophenylchlorocarbene

There total 3 articles about p-cyanophenylchlorocarbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 623-26-7
terephthalonitrile

: 882528-49-6
p-cyanophenylchlorocarbene

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaOCH₃ / methanol / 50 h / 20 °C

1.2: NH₄Cl / methanol / 60 h / 20 °C

2.1: LiCl; aq. NaOCl / dimethylsulfoxide; pentane / 0.67 h / 20 °C

3.1: CCl₄ / Flash photolysis

With sodium hypochlorite; sodium methylate; lithium chloride; In methanol; tetrachloromethane; dimethyl sulfoxide; pentane;
DOI:10.1021/ol060188c

Reference yield:

: 117837-77-1
p-cyanobenzamidine hydrochloride

: 882528-49-6
p-cyanophenylchlorocarbene

Guidance literature:: Multi-step reaction with 2 steps

1: LiCl; aq. NaOCl / dimethylsulfoxide; pentane / 0.67 h / 20 °C

2: CCl₄ / Flash photolysis

With sodium hypochlorite; lithium chloride; In tetrachloromethane; dimethyl sulfoxide; pentane;
DOI:10.1021/ol060188c