N-(2-O--D-lactoyl)-L-alanyl-D-isoglutamine benzyl ester trifluoroacetate

Base Information

Chemical Name:N-(2-O--D-lactoyl)-L-alanyl-D-isoglutamine benzyl ester trifluoroacetate
CAS No.:128747-55-7
Molecular Formula:C₂HF₃O₂*C₃₈H₅₃N₅O₁₂
Molecular Weight:885.889
Hs Code.:

N-(2-O-<benzyl 2-acetamido-6-O-(5-aminopentanoyl)-2,3-dideoxy-β-D-glucopyranosid-3-yl>-D-lactoyl)-L-alanyl-D-isoglutamine benzyl ester trifluoroacetate

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Chemical Property of N-(2-O--D-lactoyl)-L-alanyl-D-isoglutamine benzyl ester trifluoroacetate

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Technology Process of N-(2-O--D-lactoyl)-L-alanyl-D-isoglutamine benzyl ester trifluoroacetate

There total 6 articles about N-(2-O--D-lactoyl)-L-alanyl-D-isoglutamine benzyl ester trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27219-07-4
5-(N-tert-butyloxycarbonyl)aminopentanoic acid

: 128747-55-7
N-(2-O--D-lactoyl)-L-alanyl-D-isoglutamine benzyl ester trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 46.2 percent / DCC, DMAP / dimethylformamide / 3 h / Ambient temperature

2: 1 h / 0 °C

With dmap; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(89)85019-0

Reference yield:

: 57816-11-2,62928-83-0,75283-21-5,76498-06-1,76498-09-4
N-<2-O-(benzyl 2-acetamido-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

: 128747-55-7
N-(2-O--D-lactoyl)-L-alanyl-D-isoglutamine benzyl ester trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 46.2 percent / DCC, DMAP / dimethylformamide / 3 h / Ambient temperature

2: 1 h / 0 °C

With dmap; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(89)85019-0

Reference yield:

: 69323-67-7,75283-17-9,75283-19-1,75283-20-4,77844-55-4,79982-01-7,79982-02-8,122170-62-1,149622-73-1
benzyl 2-acetamido-3-O-(D-1-carboxyethyl)-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

: 128747-55-7
N-(2-O--D-lactoyl)-L-alanyl-D-isoglutamine benzyl ester trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) N-hydroxysuccinimide, DCC, 2.) triethylamine / 1.) 1,4-dioxane, 30 min., r.t., 2.) 1 h, r.t.

2: 80percent aq. acetic acid / 1 h / 45 °C

3: 46.2 percent / DCC, DMAP / dimethylformamide / 3 h / Ambient temperature

4: 1 h / 0 °C

With dmap; 1-hydroxy-pyrrolidine-2,5-dione; acetic acid; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(89)85019-0