4-[bis(2-chloroethyl)amino]benzoyl chloride

Base Information

• Chemical Name: 4-[bis(2-chloroethyl)amino]benzoyl chloride
• CAS No.: 15944-88-4
• Molecular Formula: C11H12 Cl3 N O
• Molecular Weight: 280.581
• Mol file: 15944-88-4.mol

Synonyms:Benzoylchloride, p-[bis(2-chloroethyl)amino]- (7CI,8CI); NSC 260470;p-[Bis(2-chloroethyl)amino]benzoyl chloride

Chemical Property of 4-[bis(2-chloroethyl)amino]benzoyl chloride

Chemical Property:

• Vapor Pressure: 2.02E-06mmHg at 25°C
• Boiling Point: 394.1°C at 760 mmHg
• Flash Point: 192.2°C
• Density: 1.338g/cm³

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-[bis(2-chloroethyl)amino]benzoyl chloride

There total 4 articles about 4-[bis(2-chloroethyl)amino]benzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.2%

→ 1H-2-[1-Methyl-4-[4-[N,N-bis(2-chloroethyl)amino]benzoylamino]imidazol-2-yl]benzimidazole-5-[N-(2-amidinoethyl)]carboxamide hydrochloride + 4-[N,N-bis(2-chloroethyl)amino]benzoyl chloride (15944-88-4)

Guidance literature:

Reference yield: 2.0%

4-{bis(2-chloroethyl)amino}benzoic acid (1141-37-3) → 4-[N,N-bis(2-chloroethyl)amino]benzoyl chloride (15944-88-4)

Guidance literature:

With thionyl chloride; triethylamine; In dichloromethane; chloroform; benzene;

Reference yield:

N-(N',N'-dimethylaminoethyl)-1-methyl-4-[1-methyl-4-aminoimidazole-2-carboxamido]imidazole-2-carboxamide + 4-{bis(2-chloroethyl)amino}benzoic acid (1141-37-3) → 4-[N,N-bis(2-chloroethyl)amino]benzoyl chloride (15944-88-4)

Guidance literature:

With thionyl chloride; triethylamine; In dichloromethane; chloroform; benzene;

upstream raw materials:

4-{bis(2-chloroethyl)amino}benzoic acid

Downstream raw materials:

N-{4-[bis-(2-chloro-ethyl)-amino]-benzoyl}-glycine ethyl ester

4-[bis-(2-chloroethyl)amino]benzoic acid hydrazide

4-[Bis-(2-chloro-ethyl)-amino]-benzoic acid 5-carbamoyl-1H-imidazol-4-yl ester

tallimustine

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