C₂₁H₂₁NO₃S

Base Information

Chemical Name:C₂₁H₂₁NO₃S
CAS No.:1527486-07-2
Molecular Formula:C₂₁H₂₁NO₃S
Molecular Weight:367.469
Hs Code.:

C<sub>21</sub>H<sub>21</sub>NO<sub>3</sub>S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₁NO₃S

Chemical Property:

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Technology Process of C₂₁H₂₁NO₃S

There total 5 articles about C₂₁H₂₁NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1527486-01-6
3-(bromomethyl)-2-hexanoyl-1-(phenylsulfonyl)indole

: 1527486-07-2
C₂₁H₂₁NO₃S

Guidance literature:: With acetamidine hydrochloride; potassium hydroxide; In tetrahydrofuran; water;

Reference yield:

: 83-34-1
3-Methylindole

: 1527486-07-2
C₂₁H₂₁NO₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane / 4 h / 0 - 20 °C

2.1: sec.-butyllithium / tetrahydrofuran; cyclohexane / 3 h / -70 - 20 °C

2.2: -70 °C

3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 8 h / Reflux

4.1: potassium hydroxide; acetamidine hydrochloride / tetrahydrofuran; water

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sec.-butyllithium; acetamidine hydrochloride; tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide; sodium hydroxide; In tetrahydrofuran; tetrachloromethane; dichloromethane; cyclohexane; water;

Reference yield:

: 58550-84-8
N-(phenylsulphonyl)-3-methylindole

: 1527486-07-2
C₂₁H₂₁NO₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: sec.-butyllithium / tetrahydrofuran; cyclohexane / 3 h / -70 - 20 °C

1.2: -70 °C

2.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 8 h / Reflux

3.1: potassium hydroxide; acetamidine hydrochloride / tetrahydrofuran; water

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sec.-butyllithium; acetamidine hydrochloride; potassium hydroxide; In tetrahydrofuran; tetrachloromethane; cyclohexane; water;