C₁₈H₁₈ClOP

Base Information

• Chemical Name: C₁₈H₁₈ClOP
• CAS No.: 136339-35-0
• Molecular Formula: C₁₈H₁₈ClOP
• Molecular Weight: 316.767
• Mol file: 136339-35-0.mol

Synonyms:

Chemical Property of C₁₈H₁₈ClOP

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₁₈ClOP

There total 1 articles about C₁₈H₁₈ClOP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-chloro-2-hexyn-1-ol (1002-37-5) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → C18H18ClOP (136339-35-0)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1016/S0040-4039(00)79759-0

Reference yield:

C18H18ClOP (136339-35-0) → C18H18IOP (136339-08-7)

Guidance literature:

With sodium iodide; In acetone;

DOI:10.1016/S0040-4039(00)79759-0

Reference yield:

C18H18ClOP (136339-35-0) → C18H19OP

Guidance literature:

Multi-step reaction with 2 steps

1: NaI / acetone

2: 3 percent / Bu₃SnH, AIBN / benzene / 2 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium iodide; In acetone; benzene;

DOI:10.1016/S0040-4039(00)79759-0

upstream raw materials:

6-chloro-2-hexyn-1-ol

chloro-diphenylphosphine

Downstream raw materials:

C₁₈H₁₈IOP

C₁₈H₁₉OP

Refernces