cyclo (Phe-m-aB-Gly-Gly-Gly-Gly)

Base Information

Chemical Name:cyclo (Phe-m-aB-Gly-Gly-Gly-Gly)
CAS No.:116459-32-6
Molecular Formula:C₂₅H₂₈N₆O₆
Molecular Weight:508.534
Hs Code.:

Synonyms:

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Chemical Property of cyclo (Phe-m-aB-Gly-Gly-Gly-Gly)

Chemical Property:

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Technology Process of cyclo (Phe-m-aB-Gly-Gly-Gly-Gly)

There total 6 articles about cyclo (Phe-m-aB-Gly-Gly-Gly-Gly) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1975-52-6
5-nitro-o-toluic acid

: 116459-32-6
cyclo (Phe-m-aB-Gly-Gly-Gly-Gly)

Guidance literature:: Multi-step reaction with 7 steps

1: thionyl chloride / 3 h / Ambient temperature

2: triethylamine / dimethylformamide / Ambient temperature

3: 83 percent / 5percent palladium on charcoal, H₂ / dimethylformamide / Ambient temperature

4: 53 percent / Et₃N / dimethylformamide; CH₂Cl₂ / 24 h / Ambient temperature

5: hydrazine hydrate / methanol / 48 h / Ambient temperature

6: 0.5 N aq. HCl / 24 h / Ambient temperature

7: (iPr)2EtN / dimethylformamide / 1.) -40 deg C, few min, 2.) 4 deg C, 3 d

With hydrogenchloride; palladium on activated charcoal; thionyl chloride; hydrogen; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 64688-68-2
2-methyl-5-nitrobenzoyl chloride

: 116459-32-6
cyclo (Phe-m-aB-Gly-Gly-Gly-Gly)

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / dimethylformamide / Ambient temperature

2: 83 percent / 5percent palladium on charcoal, H₂ / dimethylformamide / Ambient temperature

3: 53 percent / Et₃N / dimethylformamide; CH₂Cl₂ / 24 h / Ambient temperature

4: hydrazine hydrate / methanol / 48 h / Ambient temperature

5: 0.5 N aq. HCl / 24 h / Ambient temperature

6: (iPr)2EtN / dimethylformamide / 1.) -40 deg C, few min, 2.) 4 deg C, 3 d

With hydrogenchloride; palladium on activated charcoal; hydrogen; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: (H₂N)-m-aB-Gly-Gly-Gly-Gly-OEt

: 116459-32-6
cyclo (Phe-m-aB-Gly-Gly-Gly-Gly)

Guidance literature:: Multi-step reaction with 4 steps

1: 53 percent / Et₃N / dimethylformamide; CH₂Cl₂ / 24 h / Ambient temperature

2: hydrazine hydrate / methanol / 48 h / Ambient temperature

3: 0.5 N aq. HCl / 24 h / Ambient temperature

4: (iPr)2EtN / dimethylformamide / 1.) -40 deg C, few min, 2.) 4 deg C, 3 d

With hydrogenchloride; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;