C₂₀H₁₈F₃N₅O₂S

Base Information

Chemical Name:C₂₀H₁₈F₃N₅O₂S
CAS No.:1620328-40-6
Molecular Formula:C₂₀H₁₈F₃N₅O₂S
Molecular Weight:449.456
Hs Code.:

C<sub>20</sub>H<sub>18</sub>F<sub>3</sub>N<sub>5</sub>O<sub>2</sub>S

Synonyms:

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Chemical Property of C₂₀H₁₈F₃N₅O₂S

Chemical Property:

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Technology Process of C₂₀H₁₈F₃N₅O₂S

There total 16 articles about C₂₀H₁₈F₃N₅O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1629023-69-3
C₃₉H₃₂F₃N₅O₂S

: 1620328-40-6
C₂₀H₁₈F₃N₅O₂S

Guidance literature:: With N-tris(hydroxymethyl)methyl-2-aminoethanesulfonic acid; trifluoroacetic acid; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1016/j.bmcl.2014.05.082

Reference yield:

: 1620328-45-1
C₃₈H₂₉F₃N₄O

: 1620328-40-6
C₂₀H₁₈F₃N₅O₂S

Guidance literature:: Multi-step reaction with 4 steps

1: diphenyl phosphoryl azide; triphenylphosphine; di-isopropyl azodicarboxylate / 16 h / 0 - 20 °C

2: hydrogen; palladium 10% on activated carbon / methanol; ethyl acetate / 1 h / 20 °C

3: triethylamine / dichloromethane / 2 h / 20 °C

4: N-tris(hydroxymethyl)methyl-2-aminoethanesulfonic acid; trifluoroacetic acid / dichloromethane / 2 h / 0 °C

With di-isopropyl azodicarboxylate; N-tris(hydroxymethyl)methyl-2-aminoethanesulfonic acid; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; triethylamine; triphenylphosphine; trifluoroacetic acid; In methanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2014.05.082

Reference yield:

: 1620328-25-7
C₄₀H₃₁F₃N₄O₂

: 1620328-40-6
C₂₀H₁₈F₃N₅O₂S

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / tetrahydrofuran; methanol / 1 h / 0 °C

2: diphenyl phosphoryl azide; triphenylphosphine; di-isopropyl azodicarboxylate / 16 h / 0 - 20 °C

3: hydrogen; palladium 10% on activated carbon / methanol; ethyl acetate / 1 h / 20 °C

4: triethylamine / dichloromethane / 2 h / 20 °C

5: N-tris(hydroxymethyl)methyl-2-aminoethanesulfonic acid; trifluoroacetic acid / dichloromethane / 2 h / 0 °C

With di-isopropyl azodicarboxylate; N-tris(hydroxymethyl)methyl-2-aminoethanesulfonic acid; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; triethylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2014.05.082