4-nitrobenzeneselenenyl chloride

Base Information

• Chemical Name: 4-nitrobenzeneselenenyl chloride
• CAS No.: 57878-23-6
• Molecular Formula: C₆H₄ClNO₂Se
• Molecular Weight: 236.516
• Mol file: 57878-23-6.mol

Synonyms:

Chemical Property of 4-nitrobenzeneselenenyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-nitrobenzeneselenenyl chloride

There total 2 articles about 4-nitrobenzeneselenenyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-nitrophenyl selenocyanate (19188-18-2) → 4-nitrobenzeneselenenyl chloride (57878-23-6)

Guidance literature:

With sulfuryl dichloride; In tetrachloromethane;

DOI:10.1021/jo00171a002

Reference yield:

4-nitro-aniline (100-01-6,104810-17-5) → 4-nitrobenzeneselenenyl chloride (57878-23-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) 20percent H₂SO₄, NaNO₂, NaOAc / 4 deg C, 2) water, 48 h, r.t.

2: SO₂Cl₂ / CCl₄

With sulfuryl dichloride; sulfuric acid; sodium acetate; sodium nitrite; In tetrachloromethane;

DOI:10.1021/jo00171a002

Reference yield: 75.0%

tolyl vinyl sulfone (5535-52-4) + 4-nitrobenzeneselenenyl chloride (57878-23-6) → C15H14ClNO4SSe

Guidance literature:

In chloroform; for 15h; Heating;

upstream raw materials:

p-nitrophenyl selenocyanate

4-nitro-aniline

Downstream raw materials:

β-(4-nitrophenylseleno)ethyl chloride

1-((E)-2-Chloro-vinylselanyl)-4-nitro-benzene

4-nitrophenyl vinyl selenide