7β-hydroxynorlongifolane

Base Information

Chemical Name:7β-hydroxynorlongifolane
CAS No.:113159-74-3
Molecular Formula:C₁₄H₂₄O
Molecular Weight:208.344
Hs Code.:

Synonyms:

Suppliers and Price of 7β-hydroxynorlongifolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7β-hydroxynorlongifolane

Chemical Property:

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Technology Process of 7β-hydroxynorlongifolane

There total 8 articles about 7β-hydroxynorlongifolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73004-05-4,73068-36-7
7β-acetylnorlongifolane

: 475-23-0,113159-74-3
7β-hydroxynorlongifolane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In 1,2-dichloro-ethane; for 16h; Heating;

Reference yield:

: 113105-48-9
7β-ethynylnorlongifolane

: 475-23-0,113159-74-3
7β-hydroxynorlongifolane

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / mercuric oxide (yellow), conc. H₂SO₄ / H₂O; methanol / 16 h / Heating

2: m-chloroperbenzoic acid / 1,2-dichloro-ethane / 16 h / Heating

With sulfuric acid; 3-chloro-benzenecarboperoxoic acid; mercury(II) oxide; In methanol; water; 1,2-dichloro-ethane;

Reference yield:

: 71493-09-9,113159-73-2
3-chloro-7β-chloroethynylnorlongifolane

: 475-23-0,113159-74-3
7β-hydroxynorlongifolane

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / sodium metal / tetrahydrofuran; 2-methyl-propan-2-ol / 48 h / Heating

2: 84 percent / mercuric oxide (yellow), conc. H₂SO₄ / H₂O; methanol / 16 h / Heating

3: m-chloroperbenzoic acid / 1,2-dichloro-ethane / 16 h / Heating

With sulfuric acid; sodium; 3-chloro-benzenecarboperoxoic acid; mercury(II) oxide; In tetrahydrofuran; methanol; water; 1,2-dichloro-ethane; tert-butyl alcohol;