4,4-bis(triphenylphosphine)-arachno-4-palladanonaborane

Base Information

• Chemical Name: 4,4-bis(triphenylphosphine)-arachno-4-palladanonaborane
• CAS No.: 477773-56-1
• Molecular Formula: C₃₆H₄₂B₈P₂Pd
• Molecular Weight: 729.585
• Mol file: 477773-56-1.mol

Synonyms:

Chemical Property of 4,4-bis(triphenylphosphine)-arachno-4-palladanonaborane

Chemical Property:

Purity/Quality:

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Technology Process of 4,4-bis(triphenylphosphine)-arachno-4-palladanonaborane

There total 1 articles about 4,4-bis(triphenylphosphine)-arachno-4-palladanonaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

bis(triphenylphosphine)palladium(II) chloride (15604-37-2,13965-03-2,28966-81-6) + K(1+)*{B9H14}(1-)=K{B9H14} → 4,4-bis(triphenylphosphine)-arachno-4-palladanonaborane (477773-56-1)

Guidance literature:

In methanol; Pd complex added quickly to a stirred soln. of KB9H14 in dry MeOH, stirred at room temp. for 30 min; the solid filtered off and washed with a small quantity of MeOH, dried;

DOI:10.1016/S0022-328X(02)01552-8

upstream raw materials:

bis(triphenylphosphine)palladium(II) chloride