2,2-di(1-naphthyl)-6-phenyl-4,4-tetramethylene-1,3-dioxa-4-azonia-2-boratacyclohexane

Base Information

• Chemical Name: 2,2-di(1-naphthyl)-6-phenyl-4,4-tetramethylene-1,3-dioxa-4-azonia-2-boratacyclohexane
• CAS No.: 95890-61-2
• Molecular Formula: C₃₂H₃₀BNO₂
• Molecular Weight: 471.407
• Mol file: 95890-61-2.mol

Synonyms:

Chemical Property of 2,2-di(1-naphthyl)-6-phenyl-4,4-tetramethylene-1,3-dioxa-4-azonia-2-boratacyclohexane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2-di(1-naphthyl)-6-phenyl-4,4-tetramethylene-1,3-dioxa-4-azonia-2-boratacyclohexane

There total 1 articles about 2,2-di(1-naphthyl)-6-phenyl-4,4-tetramethylene-1,3-dioxa-4-azonia-2-boratacyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

B-(2-aminoethoxy)di(1-naphthyl)borane (6962-88-5) + N-(2-hydroxy-2-phenylethyl)pyrrolidine N-oxide (14746-43-1) → 2,2-di(1-naphthyl)-6-phenyl-4,4-tetramethylene-1,3-dioxa-4-azonia-2-boratacyclohexane (95890-61-2)

Guidance literature:

In ethanol; an EtOH soln. of amine oxide was combined with boiling ethanolic soln. of 1 equiv of borane; cooled, crystals were washed with hot ethanol, recrystd. from ethanol; elem. anal.;

DOI:10.1016/0022-328X(84)80698-1

Reference yield: 89.0%

2,2-di(1-naphthyl)-6-phenyl-4,4-tetramethylene-1,3-dioxa-4-azonia-2-boratacyclohexane (95890-61-2) → 2-(1-naphthyloxy)-2-(1-naphthyl)-5-phenyl-3,3-tetramethylen-1-oxa-3-azonia-2-boratacyclopentane (95890-70-3)

Guidance literature:

In melt; borate was heated to melting point under exclusion of moisture; melt was cooled, treated with anhyd. ether, recrystd. from benzene-ether; elem. anal.;

DOI:10.1016/0022-328X(84)80698-1

upstream raw materials:

B-(2-aminoethoxy)di(1-naphthyl)borane

N-(2-hydroxy-2-phenylethyl)pyrrolidine N-oxide

Downstream raw materials:

2-(1-naphthyloxy)-2-(1-naphthyl)-5-phenyl-3,3-tetramethylen-1-oxa-3-azonia-2-boratacyclopentane