Technology Process of C30H28(3)H2N2O4
There total 4 articles about C30H28(3)H2N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 85 percent / triethylamine; tritium / Pd/BaSO4 / dioxane / 2.5 h / 300.02 Torr
2: K2CO3; KI / acetonitrile / 2 h / 85 °C
3: toluenesulfonic acid / ethyl acetate; methanol / 2 h
4: Na2CO3; NH2OH*HCl / methanol; H2O / 2 h / 100 °C
With
tritium; o-toluenesulfonic acid; hydroxylamine hydrochloride; sodium carbonate; potassium carbonate; triethylamine; potassium iodide;
Pd-BaSO4;
In
1,4-dioxane; methanol; water; ethyl acetate; acetonitrile;
DOI:10.1002/jlcr.661
- Guidance literature:
-
With
hydroxylamine hydrochloride; sodium carbonate;
In
methanol;
at 100 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: K2CO3; KI / acetonitrile / 2 h / 85 °C
2: toluenesulfonic acid / ethyl acetate; methanol / 2 h
3: Na2CO3; NH2OH*HCl / methanol; H2O / 2 h / 100 °C
With
o-toluenesulfonic acid; hydroxylamine hydrochloride; sodium carbonate; potassium carbonate; potassium iodide;
In
methanol; water; ethyl acetate; acetonitrile;
DOI:10.1002/jlcr.661