(CO)3(CNC(CH₃)3)2ReOC₆H₄CH₃

Base Information

Chemical Name:(CO)3(CNC(CH₃)3)2ReOC₆H₄CH₃
CAS No.:146571-76-8
Molecular Formula:C₂₀H₂₅N₂O₄Re
Molecular Weight:543.636
Hs Code.:

(CO)3(CNC(CH<sub>3</sub>)3)2ReOC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>

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Suppliers and Price of (CO)3(CNC(CH₃)3)2ReOC₆H₄CH₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (CO)3(CNC(CH₃)3)2ReOC₆H₄CH₃

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Technology Process of (CO)3(CNC(CH₃)3)2ReOC₆H₄CH₃

There total 1 articles about (CO)3(CNC(CH₃)3)2ReOC₆H₄CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 138695-26-8
Re(CO)3(P(C₆H₅)3)2(OC₆H₄CH₃)

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 146571-76-8
(CO)3(CNC(CH₃)3)2ReOC₆H₄CH₃

Guidance literature:: In benzene; byproducts: P(C6H5)3; charging a bomb with Re-compound and C6H6; vac.-transfer of tert-butyl isocyanide into the bomb at -196°C; heating to 45°C for 18 h; inert atm.; removing of benzene by lyophilization;; slurrying in hexane; filtration; washing with hexane; dissolving in toluene; layering with pentane; cooling to -40°C for 2 days; crystn.; filtration; washing with hexane; further recrystn.; drying in high vac. for 12 h; elem. anal.;;
DOI:10.1021/om00027a031