(1S,3R,4R,6S)-1,4-diazidocyclohexane-3-ol-6-acetate

Base Information

Chemical Name:(1S,3R,4R,6S)-1,4-diazidocyclohexane-3-ol-6-acetate
CAS No.:864862-19-1
Molecular Formula:C₈H₁₂N₆O₃
Molecular Weight:240.222
Hs Code.:

Synonyms:

Suppliers and Price of (1S,3R,4R,6S)-1,4-diazidocyclohexane-3-ol-6-acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,3R,4R,6S)-1,4-diazidocyclohexane-3-ol-6-acetate

Chemical Property:

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Technology Process of (1S,3R,4R,6S)-1,4-diazidocyclohexane-3-ol-6-acetate

There total 4 articles about (1S,3R,4R,6S)-1,4-diazidocyclohexane-3-ol-6-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16063-09-5
(1S,3S,5R,7R)-4,8-dioxa-tricyclo[5.1.0.0]octane

: 864862-19-1
(1S,3R,4R,6S)-1,4-diazidocyclohexane-3-ol-6-acetate

Guidance literature:: Multi-step reaction with 4 steps

1: (R,R)-(salen)Cr(III)Cl complex / diethyl ether / 96 h

2: 183 mg / TFA / methanol / 0.5 h

3: 82 percent / Et₃N; dimethylaminopyridine / 1.5 h

4: 46 percent / Porcine liver esterase / dimethylsulfoxide; various solvent(s) / 16 h / pH 7.5

With porcine liver esterase; dmap; triethylamine; trifluoroacetic acid; (R,R)-(salen)Cr(III)Cl; In methanol; diethyl ether; dimethyl sulfoxide;
DOI:10.1039/b505865a

Reference yield:

: 1165952-92-0
cyclohexa-1,4-diene

: 864862-19-1
(1S,3R,4R,6S)-1,4-diazidocyclohexane-3-ol-6-acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: H₂O₂; pyridine / MeReO₃ / CH₂Cl₂

1.2: 75 percent / MnO₂ / CH₂Cl₂

2.1: (R,R)-(salen)Cr(III)Cl complex / diethyl ether / 96 h

3.1: 183 mg / TFA / methanol / 0.5 h

4.1: 82 percent / Et₃N; dimethylaminopyridine / 1.5 h

5.1: 46 percent / Porcine liver esterase / dimethylsulfoxide; various solvent(s) / 16 h / pH 7.5

With pyridine; porcine liver esterase; dmap; dihydrogen peroxide; triethylamine; trifluoroacetic acid; (R,R)-(salen)Cr(III)Cl; methyltrioxorhenium(VII); In methanol; diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1039/b505865a

Reference yield:

: (1R,2R,4S,5S)-1,4-Diazido-2,5-bis-trimethylsilanyloxy-cyclohexane

: 864862-19-1
(1S,3R,4R,6S)-1,4-diazidocyclohexane-3-ol-6-acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 183 mg / TFA / methanol / 0.5 h

2: 82 percent / Et₃N; dimethylaminopyridine / 1.5 h

3: 46 percent / Porcine liver esterase / dimethylsulfoxide; various solvent(s) / 16 h / pH 7.5

With porcine liver esterase; dmap; triethylamine; trifluoroacetic acid; In methanol; dimethyl sulfoxide;
DOI:10.1039/b505865a