(+/-)-7-deoxynimbidiol

Base Information

Chemical Name:(+/-)-7-deoxynimbidiol
CAS No.:96979-25-8
Molecular Formula:C₁₇H₂₄O₂
Molecular Weight:260.376
Hs Code.:

Synonyms:

Suppliers and Price of (+/-)-7-deoxynimbidiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-7-deoxynimbidiol

Chemical Property:

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Technology Process of (+/-)-7-deoxynimbidiol

There total 1 articles about (+/-)-7-deoxynimbidiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4698-08-2
(E)-geranic acid

: 96979-25-8,144581-66-8
(+/-)-7-deoxynimbidiol

Guidance literature:: Multi-step reaction with 8 steps

1: 82 percent / phosphate acid / toluene / 2 h / 100 °C

2: 91 percent / K₂CO₃ / acetone / 5 h / 20 °C

3: 85 percent / LiAlH₄ / diethyl ether / 4 h / 20 °C

4: 55 percent / pyridine chromium trioxide chloride / CH₂Cl₂ / 4 h / 20 °C

5: 74.5 percent / n-BuLi / tetrahydrofuran / 6 h / 20 °C

6: 100 percent / H₂ / Pd/C / diethyl ether / 0.5 h

7: boron trifluoride etherate / CH₂Cl₂ / 24 h / 20 °C

8: 76.3 percent / boron tribromide / CH₂Cl₂ / 2 h / 0 - 5 °C

With lithium aluminium tetrahydride; n-butyllithium; phosphate acid; boron trifluoride diethyl etherate; hydrogen; boron tribromide; potassium carbonate; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; toluene;
DOI:10.1016/j.bmcl.2005.11.023

Reference yield: 35.0%

: 96979-25-8,144581-66-8
(+/-)-7-deoxynimbidiol

: 113332-25-5,121702-99-6
(+/-)-nimbidiol

Guidance literature:: With sodium periodate; ruthenium trichloride; In tetrachloromethane; water; acetonitrile; at 20 - 25 ℃;
DOI:10.1016/S0040-4020(01)88267-3