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[PdCl(dimethylphenylphosphine)(2-(p-tolyl)pyridine(1-))]

Base Information
  • Chemical Name:[PdCl(dimethylphenylphosphine)(2-(p-tolyl)pyridine(1-))]
  • CAS No.:813434-38-7
  • Molecular Formula:C20H21ClNPPd
  • Molecular Weight:448.24
  • Hs Code.:
[PdCl(dimethylphenylphosphine)(2-(p-tolyl)pyridine<sup>(1-)</sup>)]

Synonyms:

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Chemical Property of [PdCl(dimethylphenylphosphine)(2-(p-tolyl)pyridine(1-))]
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Technology Process of [PdCl(dimethylphenylphosphine)(2-(p-tolyl)pyridine(1-))]

There total 1 articles about [PdCl(dimethylphenylphosphine)(2-(p-tolyl)pyridine(1-))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In tetrahydrofuran; (N2 or Ar); using Schlenk techniques; addn. of CH2Cl2 and soln. of PMe2Ph (2 equiv.) in THF to (PdCl(MeC6H3C5H4N))2; stirring for 1 h; evapn., recrystn. from CH2Cl2-hexane;
DOI:10.1039/b411432a
Guidance literature:
In dichloromethane; water; (N2 or Ar); using Schlenk techniques; addn. of CH2Cl2 and soln. of NaN3 in H2O to PdCl(MeC6H3C5H4N)(PMe2Ph); stirring for 18 h at room temp.; evapn. of solvent, extn. with CH2Cl2, recrystn. from CH2Cl2-hexane; elem. anal.;
DOI:10.1039/b411432a
Guidance literature:
Multi-step reaction with 2 steps
1: water; dichloromethane
2: dichloromethane
In dichloromethane; water;
DOI:10.1039/b411432a
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