Technology Process of C17H27NO*C20H18O8
There total 7 articles about C17H27NO*C20H18O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: n-butyllithium / tetrahydrofuran / 3 h / -60 - -55 °C
2: sodium tetrahydroborate / methanol / 25 - 35 °C
3: ethanol / 25 - 35 °C
With
sodium tetrahydroborate; n-butyllithium;
In
tetrahydrofuran; methanol; ethanol;
DOI:10.13005/ojc/340246
- Guidance literature:
-
Multi-step reaction with 7 steps
1: n-butyllithium / tetrahydrofuran / -65 °C
2: ethyl acetate / 25 - 35 °C
3: (2S,3S)-di-4-toluoyltartaric acid / ethanol / 20 h / 25 - 35 °C / Resolution of racemate
4: decalin / 190 - 195 °C
5: n-butyllithium / tetrahydrofuran / 3 h / -60 - -55 °C
6: sodium tetrahydroborate / methanol / 25 - 35 °C
7: ethanol / 25 - 35 °C
With
sodium tetrahydroborate; n-butyllithium; (2S,3S)-di-4-toluoyltartaric acid;
In
tetrahydrofuran; methanol; ethanol; ethyl acetate; decalin;
DOI:10.13005/ojc/340246
- Guidance literature:
-
Multi-step reaction with 7 steps
1: n-butyllithium / tetrahydrofuran / -65 °C
2: ethyl acetate / 25 - 35 °C
3: (2S,3S)-di-4-toluoyltartaric acid / ethanol / 20 h / 25 - 35 °C / Resolution of racemate
4: decalin / 190 - 195 °C
5: n-butyllithium / tetrahydrofuran / 3 h / -60 - -55 °C
6: sodium tetrahydroborate / methanol / 25 - 35 °C
7: ethanol / 25 - 35 °C
With
sodium tetrahydroborate; n-butyllithium; (2S,3S)-di-4-toluoyltartaric acid;
In
tetrahydrofuran; methanol; ethanol; ethyl acetate; decalin;
DOI:10.13005/ojc/340246
