(2R,2'R)-2--1-butanol

Base Information

Chemical Name:(2R,2'R)-2--1-butanol
CAS No.:105157-80-0
Molecular Formula:C₁₄H₂₃NO
Molecular Weight:221.343
Hs Code.:

(2R,2'R)-2-<N-(2'-Phenylbutyl)-amino>-1-butanol

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Suppliers and Price of (2R,2'R)-2--1-butanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,2'R)-2--1-butanol

Chemical Property:

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Technology Process of (2R,2'R)-2--1-butanol

There total 3 articles about (2R,2'R)-2--1-butanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105157-72-0
(2R,2'R)-2--1-butanol

: 105157-80-0
(2R,2'R)-2--1-butanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 8h; Yield given; Heating;
DOI:10.1002/ardp.19863190711

Reference yield:

: 938-79-4
(2R)-2-phenylbutanoic acid

: 105157-80-0
(2R,2'R)-2--1-butanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₃N, Cl-COOCH₃ / 1.) CH₂Cl₂, -15 deg C, 1 h, 2.) 0 deg C, 2 h; r.t., 4 h

2: LiAlH₄ / tetrahydrofuran / 8 h / Heating

With lithium aluminium tetrahydride; triethylamine; methyl chloroformate; In tetrahydrofuran;
DOI:10.1002/ardp.19863190711

Reference yield:

: 105227-22-3
(R)-(-)-2-phenylbutyric acid chloride

: 105157-80-0
(2R,2'R)-2--1-butanol

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Na₂CO₃ / benzene; H₂O / 1.) 10 deg C, 4 h, 2.) r.t., 4 h

2: LiAlH₄ / tetrahydrofuran / 8 h / Heating

With lithium aluminium tetrahydride; sodium carbonate; In tetrahydrofuran; water; benzene;
DOI:10.1002/ardp.19863190711