C₂₈H₄₆O₈Si

Base Information

Chemical Name:C₂₈H₄₆O₈Si
CAS No.:1313484-26-2
Molecular Formula:C₂₈H₄₆O₈Si
Molecular Weight:538.754
Hs Code.:

C<sub>28</sub>H<sub>46</sub>O<sub>8</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₄₆O₈Si

Chemical Property:

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Technology Process of C₂₈H₄₆O₈Si

There total 5 articles about C₂₈H₄₆O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313484-27-3
C₂₈H₄₆O₈Si

: 1313484-41-1
C₂₈H₄₆O₈Si

: 1313484-26-2
C₂₈H₄₆O₈Si

Guidance literature:: With lithium hexamethyldisilazane; In toluene; at -78 - 65 ℃; for 61h; optical yield given as %de; Inert atmosphere;
DOI:10.1039/c1cc11388g

Reference yield:

: 1313484-40-0
C₁₇H₃₀O₄Si

: 1313484-41-1
C₂₈H₄₆O₈Si

: 1313484-26-2
C₂₈H₄₆O₈Si

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C

2: N-ethyl-N,N-diisopropylamine; sodium iodide / tetrahydrofuran / 21 h / 20 - 50 °C / Inert atmosphere

3: lithium hexamethyldisilazane / toluene / 61 h / -78 - 65 °C / Inert atmosphere

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; toluene; 3: Ireland-Claisen rearrangement;
DOI:10.1039/c1cc11388g

Reference yield:

: 1313484-60-4
C₂₄H₃₈O₆Si

: 1313484-41-1
C₂₈H₄₆O₈Si

: 1313484-26-2
C₂₈H₄₆O₈Si

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; sodium iodide / tetrahydrofuran / 21 h / 20 - 50 °C / Inert atmosphere

2: lithium hexamethyldisilazane / toluene / 61 h / -78 - 65 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; toluene; 2: Ireland-Claisen rearrangement;
DOI:10.1039/c1cc11388g