[(WAY₄-Cp)Re(CO)3]

Base Information

Chemical Name:[(WAY₄-Cp)Re(CO)3]
CAS No.:502445-21-8
Molecular Formula:C₂₄H₂₇N₂O₅Re
Molecular Weight:609.696
Hs Code.:

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Chemical Property of [(WAY₄-Cp)Re(CO)3]

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Technology Process of [(WAY₄-Cp)Re(CO)3]

There total 2 articles about [(WAY₄-Cp)Re(CO)3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 14220-21-4
rhenium(I) pentacarbonyl bromide

: Na[WAY₄-Cp]

: 502445-21-8
[(WAY₄-Cp)Re(CO)3]

Guidance literature:: In benzene; using Schlenk techniques; Re-contg. compd. (0.155 mmol) and a ligand (0.221 mmol) were refluxed overnight in benzene soln.; evapn. of the solvent; the residue was dissolved in a min. amt. of CH2Cl2-MeOH and transferred to a silica gel column; elution with 20:1 CH2Cl2-MeOH; TLC (7:1 CH2Cl2-MeOH); HPLC (retention time 21.15 min); (1)H NMR spectra;
DOI:10.1021/ic0204575

Reference yield:

: (NEt₄)2[rhenium(I)(bromide)3(carbonyl)3]

: Na[WAY₄-Cp]

: 7732-18-5
water

: 502445-21-8
[(WAY₄-Cp)Re(CO)3]

Guidance literature:: In water; using Schlenk techniques; an aq. soln. of a ligand (0.2 mmol) was added to an aq. soln. of Re-contg. compd. (0.13 mmol); the soln. was warmed to65°C overnight; HPLC, (1)H NMR spectra;
DOI:10.1021/ic0204575