Technology Process of C22H13(2)H4NO
There total 7 articles about C22H13(2)H4NO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; copper(II) acetate monohydrate;
In
tert-Amyl alcohol;
at 100 ℃;
for 22h;
Inert atmosphere;
DOI:10.1002/anie.201101943
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C
1.2: -78 - 20 °C
2.1: N,N-dimethyl-formamide; oxalyl dichloride / ethyl acetate / 5 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
3.1: potassium carbonate / ethyl acetate; water / 10 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
4.1: potassium carbonate; [Cp*Rh(CH3CN)3](BF4)2 / water / 16 h / 110 °C / 760.05 Torr / Sealed tube; Schlenk technique
With
n-butyllithium; oxalyl dichloride; [Cp*Rh(CH3CN)3](BF4)2; potassium carbonate; N,N-dimethyl-formamide;
In
tetrahydrofuran; hexane; water; ethyl acetate;
DOI:10.1039/c7gc01221g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide; oxalyl dichloride / ethyl acetate / 5 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
2: potassium carbonate / ethyl acetate; water / 10 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
3: potassium carbonate; [Cp*Rh(CH3CN)3](BF4)2 / water / 16 h / 110 °C / 760.05 Torr / Sealed tube; Schlenk technique
With
oxalyl dichloride; [Cp*Rh(CH3CN)3](BF4)2; potassium carbonate; N,N-dimethyl-formamide;
In
water; ethyl acetate;
DOI:10.1039/c7gc01221g
