tetrabutylammonium[Ru(4,4'-bis(p-methoxystyryl)-2,2'-bipyridine)(4,4'-dicarboxy-2,2'-bipyridine)(NCS)2]

Base Information

Chemical Name:tetrabutylammonium[Ru(4,4'-bis(p-methoxystyryl)-2,2'-bipyridine)(4,4'-dicarboxy-2,2'-bipyridine)(NCS)2]
CAS No.:886538-56-3
Molecular Formula:C₁₆H₃₆N*C₄₂H₃₁N₆O₆RuS₂
Molecular Weight:1123.42
Hs Code.:

Synonyms:

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Chemical Property of tetrabutylammonium[Ru(4,4'-bis(p-methoxystyryl)-2,2'-bipyridine)(4,4'-dicarboxy-2,2'-bipyridine)(NCS)2]

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Technology Process of tetrabutylammonium[Ru(4,4'-bis(p-methoxystyryl)-2,2'-bipyridine)(4,4'-dicarboxy-2,2'-bipyridine)(NCS)2]

There total 1 articles about tetrabutylammonium[Ru(4,4'-bis(p-methoxystyryl)-2,2'-bipyridine)(4,4'-dicarboxy-2,2'-bipyridine)(NCS)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ammonium thiocyanate

: tetra-n-butylammonium hydroxide

: 886538-57-4
Ru(4,4'-bis(p-methoxystyryl)-2,2'-bipyridine)(p-cymene)Cl₂

: 6813-38-3
2,2'-Bipyridine-4,4'-dicarboxylic acid

: 886538-56-3
tetrabutylammonium[Ru(4,4'-bis(p-methoxystyryl)-2,2'-bipyridine)(4,4'-dicarboxy-2,2'-bipyridine)(NCS)2]

Guidance literature:: In N,N-dimethyl-formamide; (N2); heating a mixt. of ruthenium complex and ligand in DMF to 140°C for 4 h in the dark, addn. of NH4NCS, heating for 4 h, cooling to room temp., evapn. of DMF, addn. of water, dissolving in methanol with ammonium salt; passing through Sephadex LH-20 column with methanol, evapn., dissolving in water, addn. of nitric acid until pH 4.8, washing ppt. with water, drying in vac.; elem. anal.;
DOI:10.1021/ja058540p