(C₆H₅CH₂)2SbSi(C₂H₅)3

Base Information

• Chemical Name: (C₆H₅CH₂)2SbSi(C₂H₅)3
• CAS No.: 24696-50-2
• Molecular Formula: C₂₀H₂₉SbSi
• Molecular Weight: 419.286
• Mol file: 24696-50-2.mol

Synonyms:

Chemical Property of (C₆H₅CH₂)2SbSi(C₂H₅)3

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (C₆H₅CH₂)2SbSi(C₂H₅)3

There total 2 articles about (C₆H₅CH₂)2SbSi(C₂H₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

Tris-triaethylsilyl-antimon (4631-57-6) + benzyl chloride (100-44-7) → (C6H5CH2)2SbSi(C2H5)3 (24696-50-2) + tribenzylstibane (5072-92-4)

Guidance literature:

With lithium; In tetrahydrofuran; byproducts: {(C2H5)3Si}2; fission with Li in 107 h, treating with benzyl chloride at 50°C, 4 h;

Reference yield: 37.8%

Tris-triaethylsilyl-antimon (4631-57-6) + benzyl chloride (100-44-7) → (C6H5CH2)2SbSi(C2H5)3 (24696-50-2) + hexaethyldisilane (1633-09-6) + tribenzylstibane (5072-92-4)

Guidance literature:

With lithium; In tetrahydrofuran; treating of Sb(Si(C2H5)3)3 with Li in THF at room temp. for 107 h, addn. of C6H5CH2Cl, at 50°C for 4 h;

Reference yield:

(C6H5CH2)2SbSi(C2H5)3 (24696-50-2) → (C6H5CH2)2SbBr3 (24696-51-3)

Guidance literature:

With bromine;

upstream raw materials:

Tris-triaethylsilyl-antimon

benzyl chloride

Downstream raw materials:

(C₆H₅CH₂)2SbBr₃