4,6-Dimethyl-1-oxidopyridin-1-ium-3-carbonitrile

Base Information

Chemical Name:4,6-Dimethyl-1-oxidopyridin-1-ium-3-carbonitrile
CAS No.:7497-35-0
Molecular Formula:C₈H₈N₂O
Molecular Weight:148.164
Hs Code.:
DSSTox Substance ID:DTXSID50407707
Nikkaji Number:J2.686.778I
NSC Number:405089
Wikidata:Q82213035

Synonyms:7497-35-0;4,6-dimethyl-1-oxidopyridin-1-ium-3-carbonitrile;NCIOpen2_003725;DTXSID50407707;NSC405089;5-Cyano-2,4-dimethylpyridine 1-oxide;NSC-405089

Suppliers and Price of 4,6-Dimethyl-1-oxidopyridin-1-ium-3-carbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 4,6-Dimethyl-1-oxidopyridin-1-ium-3-carbonitrile

Chemical Property:

XLogP3:0.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:148.063662883
Heavy Atom Count:11
Complexity:184

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=[N+](C=C1C#N)[O-])C

Technology Process of 4,6-Dimethyl-1-oxidopyridin-1-ium-3-carbonitrile

There total 3 articles about 4,6-Dimethyl-1-oxidopyridin-1-ium-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1094166-04-7
C₈H₇BrN₂O

: 7497-35-0
4,6-dimethylpyridine-3-carbonitrile N-oxide

Guidance literature:: C₈H₇BrN₂O; With TurboGrignard; In tetrahydrofuran; dichloromethane; at -60 ℃; Inert atmosphere;

With water; In tetrahydrofuran; dichloromethane; at -60 ℃;
DOI:10.1021/jo802172f

Reference yield: 90.0%

: 6623-21-8
3-cyano-4,6-dimethylpyridine

: 7497-35-0
4,6-dimethylpyridine-3-carbonitrile N-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In ethyl acetate; for 1h;
DOI:10.1007/s10593-011-0861-6

Reference yield:

: 14237-71-9
2-chloro-4,6-dimethylnicotinonitrile

: 7497-35-0
4,6-dimethylpyridine-3-carbonitrile N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; zinc / water

2: 3-chloro-benzenecarboperoxoic acid / ethyl acetate / 1 h

With hydrogenchloride; 3-chloro-benzenecarboperoxoic acid; zinc; In water; ethyl acetate;
DOI:10.1007/s10593-011-0861-6