PhGe(GeBu(n)2CH₂CH₂OEt)3

Base Information

Chemical Name:PhGe(GeBu(n)2CH₂CH₂OEt)3
CAS No.:1022948-04-4
Molecular Formula:C₄₂H₈₆Ge₄O₃
Molecular Weight:929.503
Hs Code.:

PhGe(GeBu(n)2CH<sub>2</sub>CH<sub>2</sub>OEt)3

Synonyms:

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Chemical Property of PhGe(GeBu(n)2CH₂CH₂OEt)3

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Technology Process of PhGe(GeBu(n)2CH₂CH₂OEt)3

There total 1 articles about PhGe(GeBu(n)2CH₂CH₂OEt)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 894804-36-5
Bu₂Ge(NMe₂)CH₂CH₂OEt

: 2875-92-5
phenylgermane

: 1022948-04-4
PhGe(GeBu(n)2CH₂CH₂OEt)3

Guidance literature:: In acetonitrile; byproducts: Me2NH; (N2); std. Schlenk technique; soln. of Ge-NMe2 in CH3CN was added to soln. of PhGeH3 in CH3CN; sealed; heated at 85°C for 72 h; volatiles removed (vac.); distd. in Kugelrohr oven (180°C, 0.05 torr); elem. anal.;
DOI:10.1021/om800040f

Reference yield: 43.0%

: 894804-36-5
Bu₂Ge(NMe₂)CH₂CH₂OEt

: 1022948-04-4
PhGe(GeBu(n)2CH₂CH₂OEt)3

: 1022948-07-7
PhGe(GeBu(n)2GeBu(n)2CH₂CH₂OEt)3

Guidance literature:: With (i-Bu)2AlH; In hexane; acetonitrile; benzene; byproducts: (i-Bu)2AlOEt, Me2NH; (N2); std. Schlenk technique; soln. of Al compd. (3 equiv.) in hexane was added to soln. of Ge compd. in C6H6; refluxed for 24 h; evapd. (vac.);dissolved in CH3CN; treated with soln. of Ge-NMe2 in CH3CN; sealed; hea ted at 85°C for 48 h; volatiles removed (vac.); chromd. (silica gel, Et2O/hexane, 1/20); volatiles removed (vac.); elem. anal.;
DOI:10.1021/om800040f

Reference yield: 30.0%

: 894804-38-7
Ph₂Ge(NMe₂)CH₂CH₂OEt

: 1022948-04-4
PhGe(GeBu(n)2CH₂CH₂OEt)3

: 1022948-12-4
C₆H₅Ge(Ge(C₄H₉)2Ge(C₆H₅)2CH₂CH₂OC₂H₅)3

Guidance literature:: With (i-Bu)2AlH; In hexane; acetonitrile; benzene; byproducts: (i-Bu)2AlOEt, Me2NH; (N2); std. Schlenk technique; soln. of Al compd. (3 equiv.) in hexane was added to soln. of Ge compd. in C6H6; refluxed for 24 h; evapd. (vac.);dissolved in CH3CN; treated with soln. of Ge-NMe2 in CH3CN; sealed; hea ted at 85°C for 48 h; volatiles removed (vac.); chromd. (silica gel, Et2O/hexane, 1/20); volatiles removed (vac.); distd. in Kugelrohr oven (120°C, 0.05 Torr);elem. anal.;
DOI:10.1021/om800040f