tris[2-(dimethylamino)phenyl]methoxygermane

Base Information

Chemical Name:tris[2-(dimethylamino)phenyl]methoxygermane
CAS No.:198204-40-9
Molecular Formula:C₂₅H₃₃GeN₃O
Molecular Weight:464.147
Hs Code.:

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Chemical Property of tris[2-(dimethylamino)phenyl]methoxygermane

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Technology Process of tris[2-(dimethylamino)phenyl]methoxygermane

There total 1 articles about tris[2-(dimethylamino)phenyl]methoxygermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 698-00-0
2-bromo-N,N-dimethylaniline

: tetramethoxygermanium

: 198204-40-9
tris[2-(dimethylamino)phenyl]methoxygermane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane; inert atmosphere; addn. of slight excess of BuLi (hexane) to soln. of dimethylbromoaniline (Et2O) at -78°C, stirring for 2 h, addn. of TMEDA, warming (room temp.), addn. of (MeO)4Ge (THF) at -78°C, warming (room temp.), stirring for 12 h; evapn., dilution (C6H6), filtration, concn.; NMR spectroscopy;
DOI:10.1021/om970548n

Reference yield: 77.0%

: 16853-85-3
lithium aluminium tetrahydride

: 198204-40-9
tris[2-(dimethylamino)phenyl]methoxygermane

: 198204-27-2
tris[2-(dimethylamino)phenyl]hydrogermane

Guidance literature:: In tetrahydrofuran; inert atmosphere; stirring for 11 h at room temp.; addn. of H2O, aq. NaOH, H2O, filtration, concn., recrystn. (hexane); elem. anal.;
DOI:10.1021/om970548n