(S)-3-[(2S,3R,4S,5R,6R)-7-(tert-Butyl-diphenyl-silanyloxy)-3-hydroxy-4,6-dimethyl-5-triethylsilanyloxy-2-vinyl-heptanoyl]-4-isopropyl-oxazolidin-2-one

Base Information

Chemical Name:(S)-3-[(2S,3R,4S,5R,6R)-7-(tert-Butyl-diphenyl-silanyloxy)-3-hydroxy-4,6-dimethyl-5-triethylsilanyloxy-2-vinyl-heptanoyl]-4-isopropyl-oxazolidin-2-one
CAS No.:121425-39-6
Molecular Formula:C₃₉H₆₁NO₆Si₂
Molecular Weight:696.087
Hs Code.:

(S)-3-[(2S,3R,4S,5R,6R)-7-(tert-Butyl-diphenyl-silanyloxy)-3-hydroxy-4,6-dimethyl-5-triethylsilanyloxy-2-vinyl-heptanoyl]-4-isopropyl-oxazolidin-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-[(2S,3R,4S,5R,6R)-7-(tert-Butyl-diphenyl-silanyloxy)-3-hydroxy-4,6-dimethyl-5-triethylsilanyloxy-2-vinyl-heptanoyl]-4-isopropyl-oxazolidin-2-one

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Technology Process of (S)-3-[(2S,3R,4S,5R,6R)-7-(tert-Butyl-diphenyl-silanyloxy)-3-hydroxy-4,6-dimethyl-5-triethylsilanyloxy-2-vinyl-heptanoyl]-4-isopropyl-oxazolidin-2-one

There total 1 articles about (S)-3-[(2S,3R,4S,5R,6R)-7-(tert-Butyl-diphenyl-silanyloxy)-3-hydroxy-4,6-dimethyl-5-triethylsilanyloxy-2-vinyl-heptanoyl]-4-isopropyl-oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90719-29-2
(4S)-3-((E)-2-butenoyl)-4-(1-methylethyl)-2-oxazolidinone

: 106568-13-2,121440-66-2
(2R,3R,4R)-5-((tert-butyldiphenylsilyl)oxy)-2,4-dimethyl-3-((triethylsilyl)oxy)pentanal

: 121425-39-6
(S)-3-[(2S,3R,4S,5R,6R)-7-(tert-Butyl-diphenyl-silanyloxy)-3-hydroxy-4,6-dimethyl-5-triethylsilanyloxy-2-vinyl-heptanoyl]-4-isopropyl-oxazolidin-2-one

Guidance literature:: With di-n-butylboryl trifluoromethanesulfonate; dihydrogen peroxide; triethylamine; Yield given. Multistep reaction; 1.) CH₂Cl₂, from -78 deg C to -50 deg C, 2.) pH 7;
DOI:10.1021/jo00274a008

Reference yield:

: 121425-39-6
(S)-3-[(2S,3R,4S,5R,6R)-7-(tert-Butyl-diphenyl-silanyloxy)-3-hydroxy-4,6-dimethyl-5-triethylsilanyloxy-2-vinyl-heptanoyl]-4-isopropyl-oxazolidin-2-one

: 198124-80-0
(S)-3-[(2S,3R,4R,5R,6R)-7-(tert-Butyl-diphenyl-silanyloxy)-3,5-dihydroxy-4,6-dimethyl-2-vinyl-heptanoyl]-4-isopropyl-oxazolidin-2-one

Guidance literature:: With water; toluene-4-sulfonic acid; In tetrahydrofuran;
DOI:10.1021/jo00274a008

Reference yield:

: 121425-39-6
(S)-3-[(2S,3R,4S,5R,6R)-7-(tert-Butyl-diphenyl-silanyloxy)-3-hydroxy-4,6-dimethyl-5-triethylsilanyloxy-2-vinyl-heptanoyl]-4-isopropyl-oxazolidin-2-one

: 198124-64-0
(S)-3-((S)-2-{(4R,5R,6R)-6-[(R)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-but-3-enoyl)-4-isopropyl-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: pTsOH, H₂O / tetrahydrofuran

2: pTsOH

With water; toluene-4-sulfonic acid; In tetrahydrofuran;
DOI:10.1021/jo00274a008