HC[(Ct-Bu)(N-2,6-(i-Pr)2C₆H₃)]2AlEt₂

Base Information

• Chemical Name: HC[(Ct-Bu)(N-2,6-(i-Pr)2C₆H₃)]2AlEt₂
• CAS No.: 928621-08-3
• Molecular Formula: C₃₉H₆₃AlN₂
• Molecular Weight: 586.924

Synonyms:

Chemical Property of HC[(Ct-Bu)(N-2,6-(i-Pr)2C₆H₃)]2AlEt₂

Chemical Property:

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Technology Process of HC[(Ct-Bu)(N-2,6-(i-Pr)2C₆H₃)]2AlEt₂

There total 1 articles about HC[(Ct-Bu)(N-2,6-(i-Pr)2C₆H₃)]2AlEt₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.7%

N,N′-bis(2,6-diisopropylphenyl)-2,2,6,6-tetramethylheptane-3,5-diimine + triethylaluminum (97-93-8) → HC[(Ct-Bu)(N-2,6-(i-Pr)2C6H3)]2AlEt2 (928621-08-3)

Guidance literature:

In hexane; (Ar); Schlenk technique; soln. of Et3Al in hexane was added with stirring to soln. of ligand in hexane; refluxed for 24 h; concd.; kept at -25°C overnight; elem. anal.;

DOI:10.1021/om061107j

Reference yield: 83.0%

HC[(Ct-Bu)(N-2,6-(i-Pr)2C6H3)]2AlEt2 (928621-08-3) + iodine (7553-56-2,12190-71-5,8031-47-8) → HC[(Ct-Bu)(N-2,6-(i-Pr)2C6H3)]2AlI2 (928621-09-4)

Guidance literature:

In toluene; (Ar); Schlenk technique; hot (80°C) soln. of Al compd. in toluenewas added to soln. of I2 (2 equiv.) in toluene at 80°C; stirred at room temp. for 2 h; concd.; kept at -25°C overnight; elem. anal.;

DOI:10.1021/om061107j

Reference yield:

HC[(Ct-Bu)(N-2,6-(i-Pr)2C6H3)]2AlEt2 (928621-08-3) → HC[(Ct-Bu)(N-2,6-(i-Pr)2C6H3)]2Al (928621-10-7)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene

2: K / toluene

With K; In toluene;

DOI:10.1021/om061107j

upstream raw materials:

triethylaluminum

Downstream raw materials:

HC[(Ct-Bu)(N-2,6-(i-Pr)2C₆H₃)]2AlI₂

HC[(Ct-Bu)(N-2,6-(i-Pr)2C₆H₃)]2Al

HC[(Ct-Bu)(N-2,6-(i-Pr)2C₆H₃)]2Al(OH)(H)

[(HC(C(C(CH₃)3)NC₆H₃(CH(CH₃)2)2)2)Al(NC₆H₃(CH(CH₃)2)C(CH₃)2CHCNC₆H₃(CH(CH₃)2)2)]

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