C₅₅H₁₀₇O₁₂PSi₄

Base Information

Chemical Name:C₅₅H₁₀₇O₁₂PSi₄
CAS No.:158574-45-9
Molecular Formula:C₅₅H₁₀₇O₁₂PSi₄
Molecular Weight:1103.76
Hs Code.:

C<sub>55</sub>H<sub>107</sub>O<sub>12</sub>PSi<sub>4</sub>

Synonyms:

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Chemical Property of C₅₅H₁₀₇O₁₂PSi₄

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Technology Process of C₅₅H₁₀₇O₁₂PSi₄

There total 21 articles about C₅₅H₁₀₇O₁₂PSi₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 158574-42-6
(2R,3S)-5-Benzyloxy-2-methyl-3-triethylsilanyloxy-pentanal

: 158574-45-9
C₅₅H₁₀₇O₁₂PSi₄

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) (c-C₆H₁₁)2BCl, NEt₃ / 1.) CH₂Cl₂

2: 95 percent / (n-Bu)4NF / tetrahydrofuran / 0 °C

3: 70 percent / HCO₂H/Et₂O (1:1) / 25 °C

4: 2,6-lutidine / CH₂Cl₂

5: dichlorodicyanoquinone / CH₂Cl₂; H₂O

6: 1.) pyridine / 1.) 0 deg C, 2.) 25 deg C

With pyridine; 2,6-dimethylpyridine; formic acid; diethyl ether; dicyclohexylboron chloride; tetrabutyl ammonium fluoride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 158574-45-9
C₅₅H₁₀₇O₁₂PSi₄

Guidance literature:: Multi-step reaction with 3 steps

1: 2,6-lutidine / CH₂Cl₂

2: dichlorodicyanoquinone / CH₂Cl₂; H₂O

3: 1.) pyridine / 1.) 0 deg C, 2.) 25 deg C

With pyridine; 2,6-dimethylpyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water;

Reference yield:

: (4R,5S)-5-[(S)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-4-hydroxy-3,3-dimethyl-dihydro-furan-2-one

: 158574-45-9
C₅₅H₁₀₇O₁₂PSi₄

Guidance literature:: Multi-step reaction with 17 steps

1: 82 percent / (n-Bu)4NI, KH / tetrahydrofuran

3: 1.) TiCl₄ / 1.) CH₂Cl₂, 2.) CH₂Cl₂, -78 deg C

4: 1.) Me₄NHB(OAc)3, 2.) TsOH / 1.) MeCN, AcOH

5: W-2 Raney Ni / ethanol

6: Swern oxidation reagent

7: hexane; CH₂Cl₂ / -78 °C

8: 100 percent / camphorsulfonic acid / acetone / 25 °C

10: 1.) Et₃N, 4-dimethylaminopyridine, 2.) KH, <18>crown-6 / 2.) THF

12: 1.) (c-C₆H₁₁)2BCl, NEt₃ / 1.) CH₂Cl₂

13: 95 percent / (n-Bu)4NF / tetrahydrofuran / 0 °C

14: 70 percent / HCO₂H/Et₂O (1:1) / 25 °C

15: 2,6-lutidine / CH₂Cl₂

16: dichlorodicyanoquinone / CH₂Cl₂; H₂O

17: 1.) pyridine / 1.) 0 deg C, 2.) 25 deg C

With pyridine; 2,6-dimethylpyridine; dmap; formic acid; 18-crown-6 ether; diethyl ether; Swern oxidation reagent; W-2 Raney Ni; camphor-10-sulfonic acid; dicyclohexylboron chloride; tetrabutyl ammonium fluoride; titanium tetrachloride; tetra-(n-butyl)ammonium iodide; potassium hydride; toluene-4-sulfonic acid; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; acetone;