⁽⁹⁹⁾TcCl₃(P(CH₃)2C₆H₅)3

Base Information

Chemical Name:⁽⁹⁹⁾TcCl₃(P(CH₃)2C₆H₅)3
CAS No.:53749-02-3
Molecular Formula:C₂₄H₃₃Cl₃P₃Tc
Molecular Weight:619.806
Hs Code.:

<sup>(99)</sup>TcCl<sub>3</sub>(P(CH<sub>3</sub>)2C<sub>6</sub>H<sub>5</sub>)3

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Chemical Property of ⁽⁹⁹⁾TcCl₃(P(CH₃)2C₆H₅)3

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Technology Process of ⁽⁹⁹⁾TcCl₃(P(CH₃)2C₆H₅)3

There total 1 articles about ⁽⁹⁹⁾TcCl₃(P(CH₃)2C₆H₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: technetium tetrachloride

: 672-66-2
Dimethyl(phenyl)phosphine

: 53749-02-3
mer-TcCl₃(dimethylphenylphosphine)3

Guidance literature:: In not given; Schlenk technique, radiation precautions;
DOI:10.1021/ic060896u

Reference yield: 58.0%

: ammonium hexafluorophosphate

: 53749-02-3
mer-TcCl₃(dimethylphenylphosphine)3

: 119818-94-9
cis(Cl),trans(P)-{TcCl₂(dimethylphenylphosphine)(2,2'-bipyridyl)} hexafluorophosphate

: 119818-97-2
cis(Cl),trans(P)-{TcCl₂(dimethylphenylphosphine)(2,2'-bipyridyl)}

Guidance literature:: With 2,2'-bipyridyl; In ethanol; (99)Tc complex and ligand were refluxed in EtOH for 30 min and evapd. to dryness, residue was dissolved in CH2Cl2 and chromd. (Sephadex LH-20), red elution band was evapd. to dryness, dissolved in MeOH and pptd. with 1 M aq. NH4PF6 soln.; after standing overnight pptn. was filtered off, yielding Tc(III) complex; elem. anal.; Tc(II) complex was obtained from green elution band;

Reference yield: 58.0%

: ammonium hexafluorophosphate

: 66-71-7
1,10-Phenanthroline

: 53749-02-3
mer-TcCl₃(dimethylphenylphosphine)3

: cis(Cl),trans(P)-{TcCl₂(dimethylphenylphosphine)(1,10-phenanthroline)} hexafluorophosphate

Guidance literature:: In ethanol; (99)Tc complex and ligand were refluxed in EtOH for 30 min and evapd. to dryness, residue was dissolved in CH2Cl2 and chromd. (Sephadex LH-20), red elution band was evapd. to dryness, dissolved in MeOH and pptd. with 1 M aq. NH4PF6 soln.; after standing overnight pptn. was filtered off, yielding Tc(III) complex;